C₅₀H₈₆O₁₂Si₃

Base Information

Chemical Name:C₅₀H₈₆O₁₂Si₃
CAS No.:1338704-11-2
Molecular Formula:C₅₀H₈₆O₁₂Si₃
Molecular Weight:963.482
Hs Code.:

C<sub>50</sub>H<sub>86</sub>O<sub>12</sub>Si<sub>3</sub>

Synonyms:C₅₀H₈₆O₁₂Si₃

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Chemical Property of C₅₀H₈₆O₁₂Si₃

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Technology Process of C₅₀H₈₆O₁₂Si₃

There total 19 articles about C₅₀H₈₆O₁₂Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1095272-57-3
C₂₃H₄₀O₇Si₂

: 1338704-08-7
C₂₇H₄₆O₅Si

: 1338704-11-2
C₅₀H₈₆O₁₂Si₃

Guidance literature:: C₂₇H₄₆O₅Si; With phenylborondichloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 ℃; for 1h;

C₂₃H₄₀O₇Si₂; In dichloromethane; at -78 ℃; for 1.5h;
DOI:10.1021/ol2024289

Reference yield:

: C₁₀H₁₈OS₂

: 1338704-11-2
C₅₀H₈₆O₁₂Si₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 25 °C

2.1: tetrahydrofuran; diethyl ether / -78 - 0 °C

3.1: tert.-butyl lithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; pentane / 0.08 h / -78 °C

3.2: 1 h / -78 °C

4.1: water; iodine; sodium hydrogencarbonate / acetonitrile / 0.08 h / 0 - 25 °C

5.1: sodium tetrahydroborate; diethyl methoxy borane / tetrahydrofuran; methanol / -78 - 0 °C

6.1: manganese(IV) oxide / dichloromethane / 3 h / 25 °C

7.1: 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1R,2R)-2-amino-1,2-diphenylethyl)thiourea; acetic acid / toluene / 72 h / 0 °C

8.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C

9.1: phenylborondichloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -78 °C

9.2: 1.5 h / -78 °C

With 2,6-dimethylpyridine; manganese(IV) oxide; sodium tetrahydroborate; 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1R,2R)-2-amino-1,2-diphenylethyl)thiourea; diethyl methoxy borane; phenylborondichloride; water; iodine; tert.-butyl lithium; sulfur trioxide pyridine complex; sodium hydrogencarbonate; acetic acid; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; toluene; acetonitrile; pentane; 9.1: Aldol addition / 9.2: Aldol addition;
DOI:10.1021/ol2024289

Reference yield:

: C₁₁H₁₈O₂S₂

: 1338704-11-2
C₅₀H₈₆O₁₂Si₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: diisobutylaluminium hydride / toluene / 2 h / -78 °C

2.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 25 °C

3.1: tetrahydrofuran; diethyl ether / -78 - 0 °C

4.1: tert.-butyl lithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; pentane / 0.08 h / -78 °C

4.2: 1 h / -78 °C

5.1: water; iodine; sodium hydrogencarbonate / acetonitrile / 0.08 h / 0 - 25 °C

6.1: sodium tetrahydroborate; diethyl methoxy borane / tetrahydrofuran; methanol / -78 - 0 °C

7.1: manganese(IV) oxide / dichloromethane / 3 h / 25 °C

8.1: 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1R,2R)-2-amino-1,2-diphenylethyl)thiourea; acetic acid / toluene / 72 h / 0 °C

9.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C

10.1: phenylborondichloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -78 °C

10.2: 1.5 h / -78 °C

With 2,6-dimethylpyridine; manganese(IV) oxide; sodium tetrahydroborate; 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1R,2R)-2-amino-1,2-diphenylethyl)thiourea; diethyl methoxy borane; phenylborondichloride; water; iodine; tert.-butyl lithium; sulfur trioxide pyridine complex; diisobutylaluminium hydride; sodium hydrogencarbonate; acetic acid; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; toluene; acetonitrile; pentane; 10.1: Aldol addition / 10.2: Aldol addition;
DOI:10.1021/ol2024289