Technology Process of (4aR,6aS,8aS,12aS,12bR,14aS,14bR)-2,2,4a,6a,9,9,12a,14a-octamethyl-1,2,3,4,4a,5,6,6a,8,8a,9,10,11,12,12a,12b,13,14,14a,14b-icosahydropicene
There total 2 articles about (4aR,6aS,8aS,12aS,12bR,14aS,14bR)-2,2,4a,6a,9,9,12a,14a-octamethyl-1,2,3,4,4a,5,6,6a,8,8a,9,10,11,12,12a,12b,13,14,14a,14b-icosahydropicene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: CrO3, Py
2: N2H4*H2O, KOH / bis-(2-hydroxy-ethyl) ether
With
pyridine; chromium(VI) oxide; potassium hydroxide; hydrazine hydrate;
In
diethylene glycol;
DOI:10.1016/0040-4020(63)80013-7
- Guidance literature:
-
With
sulfuric acid;
In
acetic acid; benzene;
at 20 ℃;
for 10h;
Product distribution;