1'α-(thymin-1-yl)-2'-O-benzoyl-3'-O-diisopropylphosphonomethyl-L-threose

Base Information

Chemical Name:1'α-(thymin-1-yl)-2'-O-benzoyl-3'-O-diisopropylphosphonomethyl-L-threose
CAS No.:849778-78-5
Molecular Formula:C₂₃H₃₁N₂O₉P
Molecular Weight:510.481
Hs Code.:

Synonyms:1'α-(thymin-1-yl)-2'-O-benzoyl-3'-O-diisopropylphosphonomethyl-L-threose

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Chemical Property of 1'α-(thymin-1-yl)-2'-O-benzoyl-3'-O-diisopropylphosphonomethyl-L-threose

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Technology Process of 1'α-(thymin-1-yl)-2'-O-benzoyl-3'-O-diisopropylphosphonomethyl-L-threose

There total 9 articles about 1'α-(thymin-1-yl)-2'-O-benzoyl-3'-O-diisopropylphosphonomethyl-L-threose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 134963-85-2
(diisopropoxyphosphoryl)methyl trifluoromethanesulfonate

: 325684-00-2
1-(2′-O-benzoyl-α-L-threofuranosyl)thymine

: 849778-78-5
1'α-(thymin-1-yl)-2'-O-benzoyl-3'-O-diisopropylphosphonomethyl-L-threose

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at -5 - 0 ℃; for 0.25h;
DOI:10.1021/acs.jmedchem.6b01260

Reference yield: 78.0%

: 849779-01-7
1α,2-O-benzoyl-3-O-(diisopropylphosphonomethyl)-L-threose

: 65-71-4,28806-14-6,691841-57-3
thymin

: 849778-78-5
1'α-(thymin-1-yl)-2'-O-benzoyl-3'-O-diisopropylphosphonomethyl-L-threose

Guidance literature:: thymin; With ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane; Heating / reflux;

1α,2-O-benzoyl-3-O-(diisopropylphosphonomethyl)-L-threose; With tin(IV) chloride; In acetonitrile; at 20 ℃; for 4h;