2-(4-fluorobenzyl)-5,6-dimethyl-3-prop-2-yn-1-ylthieno[2,3-d]pyrimidin-4(3H)-one

Base Information

• Chemical Name: 2-(4-fluorobenzyl)-5,6-dimethyl-3-prop-2-yn-1-ylthieno[2,3-d]pyrimidin-4(3H)-one
• CAS No.: 1225504-94-8
• Molecular Formula: C₁₈H₁₅FN₂OS
• Molecular Weight: 326.394

Synonyms:2-(4-fluorobenzyl)-5,6-dimethyl-3-prop-2-yn-1-ylthieno[2,3-d]pyrimidin-4(3H)-one

Chemical Property of 2-(4-fluorobenzyl)-5,6-dimethyl-3-prop-2-yn-1-ylthieno[2,3-d]pyrimidin-4(3H)-one

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Technology Process of 2-(4-fluorobenzyl)-5,6-dimethyl-3-prop-2-yn-1-ylthieno[2,3-d]pyrimidin-4(3H)-one

There total 1 articles about 2-(4-fluorobenzyl)-5,6-dimethyl-3-prop-2-yn-1-ylthieno[2,3-d]pyrimidin-4(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

C15H13FN2OS (1225504-75-5) + propargyl bromide (106-96-7) → 2-(4-fluorobenzyl)-5,6-dimethyl-4-(prop-2-yn-1-yloxy)thieno[2,3-d]pyrimidine (1225504-93-7) + 2-(4-fluorobenzyl)-5,6-dimethyl-3-prop-2-yn-1-ylthieno[2,3-d]pyrimidin-4(3H)-one (1225504-94-8)

Guidance literature:

With potassium carbonate; In acetone; for 5h; Reflux;

DOI:10.1016/j.ejmech.2009.12.075

Reference yield: 45.0%

2-(4-fluorobenzyl)-5,6-dimethyl-3-prop-2-yn-1-ylthieno[2,3-d]pyrimidin-4(3H)-one (1225504-94-8) + 1-azido-1H,1H,2H,2H-perfluorodecane (121177-79-5) → 2-(4-fluorobenzyl)-5,6-dimethyl-3-{(1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-1H-1,2,3-triazol-4-yl)methyl}-thieno[2,3-d]pyrimidin-4(3H)-one (1225505-11-2)

Guidance literature:

With copper(l) iodide; In tetrahydrofuran; at 0 - 20 ℃; for 12.3333h;

DOI:10.1016/j.ejmech.2009.12.075

upstream raw materials:

C₁₅H₁₃FN₂OS

propargyl bromide

Downstream raw materials:

2-(4-fluorobenzyl)-5,6-dimethyl-3-{(1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-1H-1,2,3-triazol-4-yl)methyl}-thieno[2,3-d]pyrimidin-4(3H)-one

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