Technology Process of C29H37Cl2N5O4
There total 10 articles about C29H37Cl2N5O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydroxylamine hydrochloride; triethylamine; HATU;
In
dichloromethane;
at 20 ℃;
for 5h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: triethylamine; HATU / dichloromethane / 12 h / 0 - 20 °C
2.1: acetic acid / toluene / 0.5 h / 100 °C
3.1: acetic acid; zinc / dichloromethane / 1 h / 20 °C
4.1: acetic acid / water / 5 h / 23 °C
5.1: triethylamine; methanesulfonyl chloride / dichloromethane / 1 h / 0 - 20 °C
5.2: 2 h / 100 °C
6.1: lithium hydroxide monohydrate / water; tetrahydrofuran / 5 h / 23 °C
7.1: triethylamine; HATU; hydroxylamine hydrochloride / dichloromethane / 5 h / 20 °C
With
lithium hydroxide monohydrate; hydroxylamine hydrochloride; acetic acid; methanesulfonyl chloride; triethylamine; HATU; zinc;
In
tetrahydrofuran; dichloromethane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: trifluoroacetic acid / dichloromethane / 20 °C
2.1: 1,4-dioxane / 5 h / Reflux
3.1: triethylamine; HATU / dichloromethane / 12 h / 0 - 20 °C
4.1: acetic acid / toluene / 0.5 h / 100 °C
5.1: acetic acid; zinc / dichloromethane / 1 h / 20 °C
6.1: acetic acid / water / 5 h / 23 °C
7.1: triethylamine; methanesulfonyl chloride / dichloromethane / 1 h / 0 - 20 °C
7.2: 2 h / 100 °C
8.1: lithium hydroxide monohydrate / water; tetrahydrofuran / 5 h / 23 °C
9.1: triethylamine; HATU; hydroxylamine hydrochloride / dichloromethane / 5 h / 20 °C
With
lithium hydroxide monohydrate; hydroxylamine hydrochloride; acetic acid; methanesulfonyl chloride; triethylamine; HATU; trifluoroacetic acid; zinc;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene;