propane dioic acid {5-{2-[2-(2-methoxy)ethoxy]ethoxy}-1,3-phenylene}bis(methylene) ester

Base Information

Chemical Name:propane dioic acid {5-{2-[2-(2-methoxy)ethoxy]ethoxy}-1,3-phenylene}bis(methylene) ester
CAS No.:358351-53-8
Molecular Formula:C₂₁H₂₈O₁₂
Molecular Weight:472.446
Hs Code.:

Synonyms:propane dioic acid {5-{2-[2-(2-methoxy)ethoxy]ethoxy}-1,3-phenylene}bis(methylene) ester

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Chemical Property of propane dioic acid {5-{2-[2-(2-methoxy)ethoxy]ethoxy}-1,3-phenylene}bis(methylene) ester

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Technology Process of propane dioic acid {5-{2-[2-(2-methoxy)ethoxy]ethoxy}-1,3-phenylene}bis(methylene) ester

There total 4 articles about propane dioic acid {5-{2-[2-(2-methoxy)ethoxy]ethoxy}-1,3-phenylene}bis(methylene) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 2033-24-1
cycl-isopropylidene malonate

: 358351-52-7
5-(3,6,9-trioxadecyl)oxy-α,α'-dihydroxy-m-xylene

: 358351-53-8
propane dioic acid {5-{2-[2-(2-methoxy)ethoxy]ethoxy}-1,3-phenylene}bis(methylene) ester

Guidance literature:: at 110 ℃; for 6h;
DOI:10.1002/1522-2675(20010516)84:5<1119::AID-HLCA1119>3.0.CO;2-3

Reference yield:

: 112-35-6,95507-80-5
triethylene glucol monomethyl ether

: 358351-53-8
propane dioic acid {5-{2-[2-(2-methoxy)ethoxy]ethoxy}-1,3-phenylene}bis(methylene) ester

Guidance literature:: Multi-step reaction with 4 steps

1: 69 percent / pyridine / CH₂Cl₂ / 0 °C

2: 88 percent / K₂CO₃ / dimethylformamide / 48 h / 80 °C

3: 88 percent / LiAlH₄ / tetrahydrofuran / 7 h / 20 °C

4: 98 percent / 6 h / 110 °C

With pyridine; lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/1522-2675(20010516)84:5<1119::AID-HLCA1119>3.0.CO;2-3

Reference yield:

: 62921-74-8,518012-62-9,58320-73-3
2-(2-(2-methoxyethoxy)ethoxy)ethyl p-toluenesulfonate

: 358351-53-8
propane dioic acid {5-{2-[2-(2-methoxy)ethoxy]ethoxy}-1,3-phenylene}bis(methylene) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / K₂CO₃ / dimethylformamide / 48 h / 80 °C

2: 88 percent / LiAlH₄ / tetrahydrofuran / 7 h / 20 °C

3: 98 percent / 6 h / 110 °C

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/1522-2675(20010516)84:5<1119::AID-HLCA1119>3.0.CO;2-3