C₂₇H₃₁N₅O₃

Base Information

Chemical Name:C₂₇H₃₁N₅O₃
CAS No.:1346243-83-1
Molecular Formula:C₂₇H₃₁N₅O₃
Molecular Weight:473.575
Hs Code.:

C<sub>27</sub>H<sub>31</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₂₇H₃₁N₅O₃

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Chemical Property of C₂₇H₃₁N₅O₃

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Technology Process of C₂₇H₃₁N₅O₃

There total 7 articles about C₂₇H₃₁N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 558-42-9
3-chloro-2-methylpropan-2-ol

: 1346243-08-0
N-(cyclopropylmethyl)-N-(3,5-dimethoxyphenyl)-3-(1H-pyrazol-4-yl)quinoxaline-6-amine

: 1346243-83-1
C₂₇H₃₁N₅O₃

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 72h;

Reference yield:

: 10272-07-8
3.5-dimethoxyaniline

: 1346243-83-1
C₂₇H₃₁N₅O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 5 °C / Inert atmosphere

3.2: 1.83 h / 5 - 20 °C

4.1: potassium phosphate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos / 1,4-dioxane; water / 80 °C / Inert atmosphere

5.1: hydrogenchloride; water / 1,4-dioxane / 70 °C

5.2: Cooling with ice

6.1: potassium carbonate / N,N-dimethyl-formamide / 72 h / 120 °C

With hydrogenchloride; potassium phosphate; water; sodium hydride; potassium carbonate; sodium t-butanolate; trichlorophosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; XPhos; In 1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 82031-32-1
7-bromo-1H-quinoxalin-2-one

: 1346243-83-1
C₂₇H₃₁N₅O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 5 °C / Inert atmosphere

3.2: 1.83 h / 5 - 20 °C

4.1: potassium phosphate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos / 1,4-dioxane; water / 80 °C / Inert atmosphere

5.1: hydrogenchloride; water / 1,4-dioxane / 70 °C

5.2: Cooling with ice

6.1: potassium carbonate / N,N-dimethyl-formamide / 72 h / 120 °C

With hydrogenchloride; potassium phosphate; water; sodium hydride; potassium carbonate; sodium t-butanolate; trichlorophosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; XPhos; In 1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;