C₇₁H₁₀₂F₅N₅O₁₆Si

Base Information

Chemical Name:C₇₁H₁₀₂F₅N₅O₁₆Si
CAS No.:220440-11-9
Molecular Formula:C₇₁H₁₀₂F₅N₅O₁₆Si
Molecular Weight:1404.69
Hs Code.:

C<sub>71</sub>H<sub>102</sub>F<sub>5</sub>N<sub>5</sub>O<sub>16</sub>Si

Synonyms:C₇₁H₁₀₂F₅N₅O₁₆Si

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Chemical Property of C₇₁H₁₀₂F₅N₅O₁₆Si

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Technology Process of C₇₁H₁₀₂F₅N₅O₁₆Si

There total 12 articles about C₇₁H₁₀₂F₅N₅O₁₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 220440-10-8
C₆₅H₁₀₃O₁₅N₅SiO

: 220440-11-9
C₇₁H₁₀₂F₅N₅O₁₆Si

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1016/S0960-894X(98)00662-3

Reference yield:

: 74163-81-8
L-Tic-OH

: 220440-11-9
C₇₁H₁₀₂F₅N₅O₁₆Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: 97 percent / NaHCO₃ / H₂O / 1.5 h / 20 °C

2.1: 89 percent / Et₃N; DMAP; isopropenyl chloroformate / CH₂Cl₂ / 1 h / 0 °C

3.1: 86 percent / H₂ / Pd/C / methanol; ethyl acetate / 3 h / 2068.65 Torr

4.1: BOP-Cl; NMM / CH₂Cl₂ / 0.5 h / -15 °C

4.2: 60 percent / NMM / CH₂Cl₂ / 6 h / 0 °C

5.1: 100 percent / MgBr₂*Et₂O / CH₂Cl₂ / 4.5 h / -20 - 0 °C

6.1: 47 percent / NMM; isopropenyl chloroformate / CH₂Cl₂ / 4 h / -15 - 20 °C

7.1: 83 percent / aq. AcOH / tetrahydrofuran / 16 h

8.1: Dess-Martin periodinane / CH₂Cl₂ / 2 h

9.1: 100 percent / 2-methyl-2-butene; NaH₂PO₄; NaClO₂ / 2-methyl-propan-2-ol; H₂O / 20 °C

10.1: 67 percent / EDC*HCl; DMAP / CH₂Cl₂ / 13 h / 0 - 20 °C

With 4-methyl-morpholine; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; Isopropenyl chloroformate; hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; magnesium bromide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol; 8.1: Dess-Martin oxidation;
DOI:10.1021/jo0105991

Reference yield:

: 79261-58-8
(S)-3,4-dihydro-1H-isoquinoline-2,3-dicarboxylic acid 2-benzyl ester

: 220440-11-9
C₇₁H₁₀₂F₅N₅O₁₆Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: 89 percent / Et₃N; DMAP; isopropenyl chloroformate / CH₂Cl₂ / 1 h / 0 °C

2.1: 86 percent / H₂ / Pd/C / methanol; ethyl acetate / 3 h / 2068.65 Torr

3.1: BOP-Cl; NMM / CH₂Cl₂ / 0.5 h / -15 °C

3.2: 60 percent / NMM / CH₂Cl₂ / 6 h / 0 °C

4.1: 100 percent / MgBr₂*Et₂O / CH₂Cl₂ / 4.5 h / -20 - 0 °C

5.1: 47 percent / NMM; isopropenyl chloroformate / CH₂Cl₂ / 4 h / -15 - 20 °C

6.1: 83 percent / aq. AcOH / tetrahydrofuran / 16 h

7.1: Dess-Martin periodinane / CH₂Cl₂ / 2 h

8.1: 100 percent / 2-methyl-2-butene; NaH₂PO₄; NaClO₂ / 2-methyl-propan-2-ol; H₂O / 20 °C

9.1: 67 percent / EDC*HCl; DMAP / CH₂Cl₂ / 13 h / 0 - 20 °C

With 4-methyl-morpholine; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; Isopropenyl chloroformate; hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; Dess-Martin periodane; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; magnesium bromide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol; 7.1: Dess-Martin oxidation;
DOI:10.1021/jo0105991