1-p-tosyloxy-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

Base Information

Chemical Name:1-p-tosyloxy-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane
CAS No.:149746-78-1
Molecular Formula:C₂₄H₃₁NO₈S
Molecular Weight:493.578
Hs Code.:

Synonyms:1-p-tosyloxy-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

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Chemical Property of 1-p-tosyloxy-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

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Technology Process of 1-p-tosyloxy-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

There total 5 articles about 1-p-tosyloxy-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 98-59-9
p-toluenesulfonyl chloride

: 149746-77-0
2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethanol

: 149746-78-1
1-p-tosyloxy-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

Guidance literature:: With pyridine; at 5 - 10 ℃; for 4h;

Reference yield:

: 73630-14-5
potassium salt of 5-methyl-2-nitrophenol

: 149746-78-1
1-p-tosyloxy-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / potassium carbonate / dimethylformamide / 2 h / 120 °C

2: H₂ / 10percent Pd/C / ethanol / 0.5 h

3: diisopropylethylamine (DIPEA) / acetonitrile / 100 °C

4: 99 percent / sodium ethoxide / ethanol / 0.25 h

5: 98 percent / pyridine / 4 h / 5 - 10 °C

With pyridine; hydrogen; sodium ethanolate; potassium carbonate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 149746-74-7
1-acetoxy-2-(5-methyl-2-nitrophenoxy)ethane

: 149746-78-1
1-p-tosyloxy-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10percent Pd/C / ethanol / 0.5 h

2: diisopropylethylamine (DIPEA) / acetonitrile / 100 °C

3: 99 percent / sodium ethoxide / ethanol / 0.25 h

4: 98 percent / pyridine / 4 h / 5 - 10 °C

With pyridine; hydrogen; sodium ethanolate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; acetonitrile;