4-methyl-N-(6-hydroxy-2-(2-methyl-1-propenyl)-8-quinolyl)benzenesulfonamide

Base Information

Chemical Name:4-methyl-N-(6-hydroxy-2-(2-methyl-1-propenyl)-8-quinolyl)benzenesulfonamide
CAS No.:316124-87-5
Molecular Formula:C₂₀H₂₀N₂O₃S
Molecular Weight:368.456
Hs Code.:

Synonyms:4-methyl-N-(6-hydroxy-2-(2-methyl-1-propenyl)-8-quinolyl)benzenesulfonamide

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Chemical Property of 4-methyl-N-(6-hydroxy-2-(2-methyl-1-propenyl)-8-quinolyl)benzenesulfonamide

Chemical Property:

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Technology Process of 4-methyl-N-(6-hydroxy-2-(2-methyl-1-propenyl)-8-quinolyl)benzenesulfonamide

There total 6 articles about 4-methyl-N-(6-hydroxy-2-(2-methyl-1-propenyl)-8-quinolyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 316124-83-1
4-methyl-N-(6-methoxy-2-(2-methyl-1-propenyl)-8-quinolyl)benzenesulfonamide

: 316124-87-5
4-methyl-N-(6-hydroxy-2-(2-methyl-1-propenyl)-8-quinolyl)benzenesulfonamide

Guidance literature:: With boron tribromide; In dichloromethane; for 4h; Heating;
DOI:10.1021/jo000678x

Reference yield:

: 54232-06-3
6-methoxy-2-methyl-8-nitroquinoline

: 316124-87-5
4-methyl-N-(6-hydroxy-2-(2-methyl-1-propenyl)-8-quinolyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: 63 percent / selenious acid / dioxane; H₂O / 1 h / Heating

2.1: sodium hydroxide / CH₂Cl₂; H₂O / 5 h

2.2: 83 percent / p-toluenesulfonic acid / ethanol / 6 h / Heating

3.1: 83 percent / iron powder; glacial acetic acid / ethanol / 3.5 h / Heating

4.1: 91 percent / pyridine / CH₂Cl₂

5.1: 98 percent / boron tribromide / CH₂Cl₂ / 4 h / Heating

With pyridine; sodium hydroxide; boron tribromide; selenious acid; iron; acetic acid; In 1,4-dioxane; ethanol; dichloromethane; water; 1.1: Mathur oxidation / 2.1: Wittig reaction;
DOI:10.1021/jo000678x

Reference yield:

: 133378-39-9
6-methoxy-8-nitroquinolinecarbaldehyde

: 316124-87-5
4-methyl-N-(6-hydroxy-2-(2-methyl-1-propenyl)-8-quinolyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / CH₂Cl₂; H₂O / 5 h

1.2: 83 percent / p-toluenesulfonic acid / ethanol / 6 h / Heating

2.1: 83 percent / iron powder; glacial acetic acid / ethanol / 3.5 h / Heating

3.1: 91 percent / pyridine / CH₂Cl₂

4.1: 98 percent / boron tribromide / CH₂Cl₂ / 4 h / Heating

With pyridine; sodium hydroxide; boron tribromide; iron; acetic acid; In ethanol; dichloromethane; water; 1.1: Wittig reaction;
DOI:10.1021/jo000678x