O-(tert-butyldiphenylsilyl)-N-<1-methyl-1-<4-(benzyloxy)phenyl>ethyl>hydroxylamine

Base Information

Chemical Name:O-(tert-butyldiphenylsilyl)-N-<1-methyl-1-<4-(benzyloxy)phenyl>ethyl>hydroxylamine
CAS No.:118684-94-9
Molecular Formula:C₃₂H₃₇NO₂Si
Molecular Weight:495.737
Hs Code.:

Synonyms:O-(tert-butyldiphenylsilyl)-N-<1-methyl-1-<4-(benzyloxy)phenyl>ethyl>hydroxylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-(tert-butyldiphenylsilyl)-N-<1-methyl-1-<4-(benzyloxy)phenyl>ethyl>hydroxylamine

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Technology Process of O-(tert-butyldiphenylsilyl)-N-<1-methyl-1-<4-(benzyloxy)phenyl>ethyl>hydroxylamine

There total 2 articles about O-(tert-butyldiphenylsilyl)-N-<1-methyl-1-<4-(benzyloxy)phenyl>ethyl>hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 94571-13-8
1-methyl-1-<4-(benzyloxy)phenyl>ethanol

: 103587-51-5
O-(tert-butyl)diphenylsilylhydroxylamine

: 118684-94-9
O-(tert-butyldiphenylsilyl)-N-<1-methyl-1-<4-(benzyloxy)phenyl>ethyl>hydroxylamine

Guidance literature:: With trifluoroacetic acid; In benzene; for 48h; Ambient temperature;
DOI:10.1021/jo00266a050

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 118684-94-9
O-(tert-butyldiphenylsilyl)-N-<1-methyl-1-<4-(benzyloxy)phenyl>ethyl>hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / hydroxylamine hydrochloride, triethylamine / CH₂Cl₂ / Ambient temperature

2: 47 percent / trifluoroacetic acid (TFA) / benzene / 48 h / Ambient temperature

With hydroxylamine hydrochloride; triethylamine; trifluoroacetic acid; In dichloromethane; benzene;
DOI:10.1021/jo00266a050