(E)-2-[8-(2-ethyl-4-phenylimidazol-1-yl)methyl-6,11-dihydrodibenzo[b,e]oxepin-11-ylidene]propiononitrile

Base Information

Chemical Name:(E)-2-[8-(2-ethyl-4-phenylimidazol-1-yl)methyl-6,11-dihydrodibenzo[b,e]oxepin-11-ylidene]propiononitrile
CAS No.:1207546-56-2
Molecular Formula:C₂₉H₂₅N₃O
Molecular Weight:431.537
Hs Code.:

Synonyms:(E)-2-[8-(2-ethyl-4-phenylimidazol-1-yl)methyl-6,11-dihydrodibenzo[b,e]oxepin-11-ylidene]propiononitrile

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Chemical Property of (E)-2-[8-(2-ethyl-4-phenylimidazol-1-yl)methyl-6,11-dihydrodibenzo[b,e]oxepin-11-ylidene]propiononitrile

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Technology Process of (E)-2-[8-(2-ethyl-4-phenylimidazol-1-yl)methyl-6,11-dihydrodibenzo[b,e]oxepin-11-ylidene]propiononitrile

There total 2 articles about (E)-2-[8-(2-ethyl-4-phenylimidazol-1-yl)methyl-6,11-dihydrodibenzo[b,e]oxepin-11-ylidene]propiononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1207547-57-6
(E)-2-{8-(chloromethyl)dibenzo[b,e]oxepin-11(6H)-ylidene}propanenitrile

: 13739-51-0
2-ethyl-4-phenyl-1H-imidazole

: 1207546-56-2
(E)-2-[8-(2-ethyl-4-phenylimidazol-1-yl)methyl-6,11-dihydrodibenzo[b,e]oxepin-11-ylidene]propiononitrile

Guidance literature:: 2-ethyl-4-phenyl-1H-imidazole; With potassium carbonate; In N,N-dimethyl-formamide; for 0.25h;

(E)-2-{8-(chloromethyl)dibenzo[b,e]oxepin-11(6H)-ylidene}propanenitrile; In N,N-dimethyl-formamide; at 60 ℃; for 3h;

Reference yield:

: 1046822-98-3
(E)-2-{8-(hydroxymethyl)dibenzo[b,e]oxepin-11(6H)-ylidene}propanenitrile

: 1207546-56-2
(E)-2-[8-(2-ethyl-4-phenylimidazol-1-yl)methyl-6,11-dihydrodibenzo[b,e]oxepin-11-ylidene]propiononitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; methanesulfonyl chloride; lithium chloride / tetrahydrofuran / 2 h / 50 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.25 h

2.2: 3 h / 60 °C

With potassium carbonate; methanesulfonyl chloride; triethylamine; lithium chloride; In tetrahydrofuran; N,N-dimethyl-formamide;