(2S,3S,4R)-1-(tert-butyldiphenylsilyloxy)-2-[N-(acetyl)amino]octadecan-3,4-cyclic Sulfite

Base Information

Chemical Name:(2S,3S,4R)-1-(tert-butyldiphenylsilyloxy)-2-[N-(acetyl)amino]octadecan-3,4-cyclic Sulfite
CAS No.:1262283-57-7
Molecular Formula:C₃₆H₅₇NO₅SSi
Molecular Weight:644.004
Hs Code.:

Synonyms:(2S,3S,4R)-1-(tert-butyldiphenylsilyloxy)-2-[N-(acetyl)amino]octadecan-3,4-cyclic Sulfite

Suppliers and Price of (2S,3S,4R)-1-(tert-butyldiphenylsilyloxy)-2-[N-(acetyl)amino]octadecan-3,4-cyclic Sulfite

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (2S,3S,4R)-1-(tert-butyldiphenylsilyloxy)-2-[N-(acetyl)amino]octadecan-3,4-cyclic Sulfite

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Hazard Codes:

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Technology Process of (2S,3S,4R)-1-(tert-butyldiphenylsilyloxy)-2-[N-(acetyl)amino]octadecan-3,4-cyclic Sulfite

There total 3 articles about (2S,3S,4R)-1-(tert-butyldiphenylsilyloxy)-2-[N-(acetyl)amino]octadecan-3,4-cyclic Sulfite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1262283-56-6
(2S,3S,4R)-1-(tert-butyldiphenylsilyloxy)-2-[N-(acetyl)amino]octadecan-3,4-diol

: 1262283-57-7
(2S,3S,4R)-1-(tert-butyldiphenylsilyloxy)-2-[N-(acetyl)amino]octadecan-3,4-cyclic Sulfite

Guidance literature:: With thionyl chloride; triethylamine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/jo101757k

Reference yield:

: 13018-48-9
N,O,O,O-tetraacetyl-D-ribo-phytosphingosine

: 1262283-57-7
(2S,3S,4R)-1-(tert-butyldiphenylsilyloxy)-2-[N-(acetyl)amino]octadecan-3,4-cyclic Sulfite

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; sodium methylate / 0.5 h / 20 °C / Inert atmosphere

2: dmap; triethylamine / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With methanol; dmap; thionyl chloride; sodium methylate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo101757k

Reference yield:

: 21830-28-4
N-acetyl-D-ribophytosphingosine

: 1262283-57-7
(2S,3S,4R)-1-(tert-butyldiphenylsilyloxy)-2-[N-(acetyl)amino]octadecan-3,4-cyclic Sulfite

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With dmap; thionyl chloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo101757k