C₅₇H₈₈O₈SSi₃

Base Information

Chemical Name:C₅₇H₈₈O₈SSi₃
CAS No.:945468-75-7
Molecular Formula:C₅₇H₈₈O₈SSi₃
Molecular Weight:1017.64
Hs Code.:

C<sub>57</sub>H<sub>88</sub>O<sub>8</sub>SSi<sub>3</sub>

Synonyms:C₅₇H₈₈O₈SSi₃

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Chemical Property of C₅₇H₈₈O₈SSi₃

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Technology Process of C₅₇H₈₈O₈SSi₃

There total 34 articles about C₅₇H₈₈O₈SSi₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 945468-74-6
C₅₈H₈₆O₉SSi₃

: 945468-75-7
C₅₇H₈₈O₈SSi₃

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at -30 ℃; for 1.5h;
DOI:10.1016/j.tetlet.2007.04.136

Reference yield:

: C₁₇H₂₄O₅

: 945468-75-7
C₅₇H₈₈O₈SSi₃

Guidance literature:: Multi-step reaction with 16 steps

1.1: 73 percent / DIBALH / CH₂Cl₂ / 0.67 h / -78 °C

2.1: (+)-diisopropyl tartrate; Ti(OiPr)4; TBHP / 4A MS / CH₂Cl₂ / 12 h / -30 °C

3.1: 100 percent / LiAlH₄ / tetrahydrofuran / 1 h / 24 °C

4.1: 95 percent / 2,6-lutidine / CH₂Cl₂ / 0.75 h / -40 °C

5.1: 89 percent / K₂CO₃ / methanol / 0.03 h / 23 °C

6.1: 87 percent / TPAP; NMO; 4A MS / CH₂Cl₂ / 0.5 h / 0 °C

7.1: NaH / benzene; tetrahydrofuran / 0.08 h / 0 °C

7.2: 85 percent / benzene; tetrahydrofuran / 8 h / -78 °C

8.1: 98 percent / NaBH₄; CeCl₃*H₂O / ethanol / 3 h / -20 °C

9.1: 93 percent / K₂CO₃ / methanol / 2 h / 24 °C

10.1: 95 percent / m-CPBA; NaHCO₃ / CH₂Cl₂ / 2 h / 0 °C

11.1: 2,6-lutidine / CH₂Cl₂ / 1 h / -20 °C

12.1: 77 percent / CSA / CH₂Cl₂ / 4 h / 0 °C

13.1: 95 percent / pyridine / CH₂Cl₂ / 2 h / 0 °C

14.1: 95 percent / TMSOTf; 2,6-lutidine / CH₂Cl₂ / 2 h / 0 °C

15.1: 94 percent / Bu₃P / CH₂Cl₂ / 1 h / 25 °C

16.1: 100 percent / LiAlH₄ / diethyl ether / 1.5 h / -30 °C

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium tetrahydroborate; lithium aluminium tetrahydride; N-methyl-2-indolinone; cerium(III) chloride; tetrapropylammonium perruthennate; L-(+)-diisopropyl tartrate; tributylphosphine; trimethylsilyl trifluoromethanesulfonate; camphor-10-sulfonic acid; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; 4A MS; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; benzene; 2.1: Katsuki-Sharpless asymmetric epoxidation / 7.1: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.tetlet.2007.04.136

Reference yield:

: 945468-63-3
C₁₅H₂₂O₄

: 945468-75-7
C₅₇H₈₈O₈SSi₃

Guidance literature:: Multi-step reaction with 15 steps

1.1: (+)-diisopropyl tartrate; Ti(OiPr)4; TBHP / 4A MS / CH₂Cl₂ / 12 h / -30 °C

2.1: 100 percent / LiAlH₄ / tetrahydrofuran / 1 h / 24 °C

3.1: 95 percent / 2,6-lutidine / CH₂Cl₂ / 0.75 h / -40 °C

4.1: 89 percent / K₂CO₃ / methanol / 0.03 h / 23 °C

5.1: 87 percent / TPAP; NMO; 4A MS / CH₂Cl₂ / 0.5 h / 0 °C

6.1: NaH / benzene; tetrahydrofuran / 0.08 h / 0 °C

6.2: 85 percent / benzene; tetrahydrofuran / 8 h / -78 °C

7.1: 98 percent / NaBH₄; CeCl₃*H₂O / ethanol / 3 h / -20 °C

8.1: 93 percent / K₂CO₃ / methanol / 2 h / 24 °C

9.1: 95 percent / m-CPBA; NaHCO₃ / CH₂Cl₂ / 2 h / 0 °C

10.1: 2,6-lutidine / CH₂Cl₂ / 1 h / -20 °C

11.1: 77 percent / CSA / CH₂Cl₂ / 4 h / 0 °C

12.1: 95 percent / pyridine / CH₂Cl₂ / 2 h / 0 °C

13.1: 95 percent / TMSOTf; 2,6-lutidine / CH₂Cl₂ / 2 h / 0 °C

14.1: 94 percent / Bu₃P / CH₂Cl₂ / 1 h / 25 °C

15.1: 100 percent / LiAlH₄ / diethyl ether / 1.5 h / -30 °C

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium tetrahydroborate; lithium aluminium tetrahydride; N-methyl-2-indolinone; cerium(III) chloride; tetrapropylammonium perruthennate; L-(+)-diisopropyl tartrate; tributylphosphine; trimethylsilyl trifluoromethanesulfonate; camphor-10-sulfonic acid; sodium hydride; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; 4A MS; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; benzene; 1.1: Katsuki-Sharpless asymmetric epoxidation / 6.1: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.tetlet.2007.04.136