Technology Process of C54H84O6S3Si3
There total 3 articles about C54H84O6S3Si3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H24O6S3;
With
lithium diisopropyl amide;
In
tetrahydrofuran;
at -78 ℃;
for 1h;
triisopropylsilyl chloride;
In
tetrahydrofuran;
at -78 - 20 ℃;
for 1h;
DOI:10.1021/ol201466z
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C
1.2: 1 h / -78 - 20 °C
1.3: Reflux
2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C
2.2: 1 h / -78 - 20 °C
With
lithium diisopropyl amide;
In
tetrahydrofuran;
1.1: Negishi coupling reaction / 1.2: Negishi coupling reaction / 1.3: Negishi coupling reaction;
DOI:10.1021/ol201466z
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C
1.2: 1 h / -78 - 20 °C
1.3: Reflux
2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C
2.2: 1 h / -78 - 20 °C
With
lithium diisopropyl amide;
In
tetrahydrofuran;
1.1: Negishi coupling reaction / 1.2: Negishi coupling reaction / 1.3: Negishi coupling reaction;
DOI:10.1021/ol201466z