{(1R,6S)-3,5,5,8,10,10-hexaphenyl-2,4,7,9-tetraoxa-3,8-diborobicyclo[4.4.0]decane}

Base Information

Chemical Name:{(1R,6S)-3,5,5,8,10,10-hexaphenyl-2,4,7,9-tetraoxa-3,8-diborobicyclo[4.4.0]decane}
CAS No.:1103686-27-6
Molecular Formula:C₄₀H₃₂B₂O₄
Molecular Weight:598.314
Hs Code.:

Synonyms:{(1R,6S)-3,5,5,8,10,10-hexaphenyl-2,4,7,9-tetraoxa-3,8-diborobicyclo[4.4.0]decane}

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Chemical Property of {(1R,6S)-3,5,5,8,10,10-hexaphenyl-2,4,7,9-tetraoxa-3,8-diborobicyclo[4.4.0]decane}

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Technology Process of {(1R,6S)-3,5,5,8,10,10-hexaphenyl-2,4,7,9-tetraoxa-3,8-diborobicyclo[4.4.0]decane}

There total 3 articles about {(1R,6S)-3,5,5,8,10,10-hexaphenyl-2,4,7,9-tetraoxa-3,8-diborobicyclo[4.4.0]decane} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 909707-20-6
(2S,3S)-1,1,4,4-tetraphenylbutane-1,2,3,4-tetraol

: 98-80-6
phenylboronic acid

: 1103686-27-6
{(1R,6S)-3,5,5,8,10,10-hexaphenyl-2,4,7,9-tetraoxa-3,8-diborobicyclo[4.4.0]decane}

Guidance literature:: In tetrahydrofuran; for 2h; Reflux;
DOI:10.1016/j.tetasy.2009.05.030

Reference yield: 50.0%

: 108-86-1,52753-63-6
bromobenzene

: (4S,5S)-4,5-bis(ethoxycarbonyl)-2-phenyl-1,3,2-dioxaborolane

: 1103686-27-6
{(1R,6S)-3,5,5,8,10,10-hexaphenyl-2,4,7,9-tetraoxa-3,8-diborobicyclo[4.4.0]decane}

Guidance literature:: bromobenzene; With magnesium; In tetrahydrofuran; Inert atmosphere;

(4S,5S)-4,5-bis(ethoxycarbonyl)-2-phenyl-1,3,2-dioxaborolane; In tetrahydrofuran; at 0 ℃; Reflux; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.05.030

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: (4S,5S)-2-butoxy-4,5-bis(ethoxycarbonyl)-1,3,2-dioxaborolane

: 1103686-27-6
{(1R,6S)-3,5,5,8,10,10-hexaphenyl-2,4,7,9-tetraoxa-3,8-diborobicyclo[4.4.0]decane}

Guidance literature:: bromobenzene; With magnesium; In tetrahydrofuran; Inert atmosphere;

(4S,5S)-2-butoxy-4,5-bis(ethoxycarbonyl)-1,3,2-dioxaborolane; In tetrahydrofuran; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.05.030