Technology Process of C55H59NO15
There total 9 articles about C55H59NO15 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C47H53NO14; p-Anisaldehyde dimethyl acetal;
toluene-4-sulfonic acid;
In
dichloromethane;
at 20 ℃;
for 0.75h;
With
sodium hydrogencarbonate;
In
dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: hydrazine / Isopropyl acetate / 1 h / 20 °C
2.1: dmap / dichloromethane / 3 h / 20 °C
3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 22 h / 20 °C
4.1: sodium tetrahydroborate / methanol; ethanol / 5 h / 0 °C
5.1: dmap / dichloromethane / 15 h / 20 °C
5.2: 0.08 h
6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C
7.1: toluene-4-sulfonic acid / dichloromethane / 0.75 h / 20 °C
With
dmap; sodium tetrahydroborate; tetrapropylammonium perruthennate; tetrabutyl ammonium fluoride; 4-methylmorpholine N-oxide; hydrazine;
toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; Isopropyl acetate;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dmap / dichloromethane / 15 h / 20 °C
1.2: 0.08 h
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C
3.1: toluene-4-sulfonic acid / dichloromethane / 0.75 h / 20 °C
With
dmap; tetrabutyl ammonium fluoride;
toluene-4-sulfonic acid;
In
tetrahydrofuran; dichloromethane;