1,11-bis[2-oxo-3-(1-phenylindolizin-2-yl)quinoxalin-1-yl]-3,6,9-trioxaundecane

Base Information

• Chemical Name: 1,11-bis[2-oxo-3-(1-phenylindolizin-2-yl)quinoxalin-1-yl]-3,6,9-trioxaundecane
• CAS No.: 917387-54-3
• Molecular Formula: C₅₂H₄₄N₆O₅
• Molecular Weight: 832.959

Synonyms:1,11-bis[2-oxo-3-(1-phenylindolizin-2-yl)quinoxalin-1-yl]-3,6,9-trioxaundecane

Chemical Property of 1,11-bis[2-oxo-3-(1-phenylindolizin-2-yl)quinoxalin-1-yl]-3,6,9-trioxaundecane

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Technology Process of 1,11-bis[2-oxo-3-(1-phenylindolizin-2-yl)quinoxalin-1-yl]-3,6,9-trioxaundecane

There total 3 articles about 1,11-bis[2-oxo-3-(1-phenylindolizin-2-yl)quinoxalin-1-yl]-3,6,9-trioxaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

3-(1-phenylindolizin-2-yl)quinoxalin-2(1H)-one (894108-15-7) + 1-bromo-2-{2-[2-(2-bromoethoxy)ethoxy]-ethoxy}ethane (31255-26-2) → 1,11-bis[2-oxo-3-(1-phenylindolizin-2-yl)quinoxalin-1-yl]-3,6,9-trioxaundecane (917387-54-3)

Guidance literature:

With potassium hydroxide; In 1,4-dioxane; for 24h; Reflux;

DOI:10.1016/j.tet.2013.09.014

Reference yield: 37.0%

3-(1-phenylindolizin-2-yl)quinoxalin-2(1H)-one (894108-15-7) + 1-bromo-2-{2-[2-(2-bromoethoxy)ethoxy]-ethoxy}ethane (31255-26-2) → 1-(11-bromo-3,6,9-trioxaundec-1-yl)-3-(1-phenylindolizin-2-yl)quinoxalin-2-one + 1,11-bis[2-oxo-3-(1-phenylindolizin-2-yl)quinoxalin-1-yl]-3,6,9-trioxaundecane (917387-54-3)

Guidance literature:

With potassium hydroxide; In 1,4-dioxane; for 12h; Heating;

DOI:10.1007/s11172-006-0165-7

Reference yield:

3-[β-(2'-benzylpyridinio)-α-hydroxyvinyl]quinoxalin-2(1H)-one iodide → 1,11-bis[2-oxo-3-(1-phenylindolizin-2-yl)quinoxalin-1-yl]-3,6,9-trioxaundecane (917387-54-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 71 percent / Et₃N / CHCl₃ / 72 h

2: 37 percent / KOH / dioxane / 12 h / Heating

With potassium hydroxide; triethylamine; In 1,4-dioxane; chloroform;

DOI:10.1007/s11172-006-0165-7

upstream raw materials:

3-(1-phenylindolizin-2-yl)quinoxalin-2(1H)-one

1-bromo-2-{2-[2-(2-bromoethoxy)ethoxy]-ethoxy}ethane

Downstream raw materials:

1²,4²-dioxo-2¹,3¹-diphenyl-7,10,13-trioxa-1,4(3,1)-diquinoxalina-2(2,3),3(3,2)-diindolizinacyclopentadecaphane

C₁₀₄H₈₄N₁₂O₁₀

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