(1S,2R,3R)-1-methyl-3-(1-methyl-1-triethylsiloxyethyl)-2-(2'-nitrophenylselanylmethyl)cyclopentane

Base Information

Chemical Name:(1S,2R,3R)-1-methyl-3-(1-methyl-1-triethylsiloxyethyl)-2-(2'-nitrophenylselanylmethyl)cyclopentane
CAS No.:162460-46-0
Molecular Formula:C₂₂H₃₇NO₃SeSi
Molecular Weight:470.586
Hs Code.:

Synonyms:(1S,2R,3R)-1-methyl-3-(1-methyl-1-triethylsiloxyethyl)-2-(2'-nitrophenylselanylmethyl)cyclopentane

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Chemical Property of (1S,2R,3R)-1-methyl-3-(1-methyl-1-triethylsiloxyethyl)-2-(2'-nitrophenylselanylmethyl)cyclopentane

Chemical Property:

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Technology Process of (1S,2R,3R)-1-methyl-3-(1-methyl-1-triethylsiloxyethyl)-2-(2'-nitrophenylselanylmethyl)cyclopentane

There total 5 articles about (1S,2R,3R)-1-methyl-3-(1-methyl-1-triethylsiloxyethyl)-2-(2'-nitrophenylselanylmethyl)cyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 79271-56-0
triethylsilyl trifluoromethyl sulfonate

: 162460-45-9
(1'R,2'R,3'S)-2-<2'-(2''-nitrophenylselanylmethyl)-3'-methylcyclopentyl>propan-2-ol

: 162460-46-0
(1S,2R,3R)-1-methyl-3-(1-methyl-1-triethylsiloxyethyl)-2-(2'-nitrophenylselanylmethyl)cyclopentane

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; for 1h; Ambient temperature;

Reference yield:

: 51694-22-5
ortho-nitrophenyl selenocyanate

: 162460-46-0
(1S,2R,3R)-1-methyl-3-(1-methyl-1-triethylsiloxyethyl)-2-(2'-nitrophenylselanylmethyl)cyclopentane

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / Bu₃P / tetrahydrofuran / 2 h / Ambient temperature

2: 100 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / Ambient temperature

With 2,6-dimethylpyridine; tributylphosphine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 2005-60-9,2078-88-8,30165-19-6,35337-16-7,35337-17-8,122045-56-1,134452-55-4
(1R,2R,5S)-2-Isopropenyl-5-methyl-cyclopentanecarboxylic acid methyl ester

: 162460-46-0
(1S,2R,3R)-1-methyl-3-(1-methyl-1-triethylsiloxyethyl)-2-(2'-nitrophenylselanylmethyl)cyclopentane

Guidance literature:: Multi-step reaction with 4 steps

1: MCPBA, KHCO₃ / CH₂Cl₂ / 2 h / 0 °C

2: LiAlH₄ / tetrahydrofuran / 4 h / Ambient temperature

3: 100 percent / Bu₃P / tetrahydrofuran / 2 h / Ambient temperature

4: 100 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / Ambient temperature

With 2,6-dimethylpyridine; lithium aluminium tetrahydride; tributylphosphine; potassium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;