3-chlorophenylisocyanic acid

Base Information

• Chemical Name: 3-chlorophenylisocyanic acid
• CAS No.: 13400-54-9
• Molecular Formula: C₇H₆ClNO₂
• Molecular Weight: 171.583

Synonyms:3-chlorophenylisocyanic acid

Chemical Property of 3-chlorophenylisocyanic acid

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

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Technology Process of 3-chlorophenylisocyanic acid

There total 4 articles about 3-chlorophenylisocyanic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

m-chlorophenyl isocyanate (2909-38-8) → 3-chlorophenylisocyanic acid (13400-54-9)

Guidance literature:

With water; at 100 ℃; for 12h; Sealed tube;

DOI:10.1016/j.tetlet.2021.153550

Reference yield:

(3-chloro-phenyl)-carbamic acid pyridin-2-ylmethyl ester (21780-36-9) → 3-chlorophenylisocyanic acid (13400-54-9)

Guidance literature:

Kinetics; acid-catalyzed hydroylsis;

Reference yield:

(3-Chloro-phenyl)-carbamic acid 2-pyridin-2-yl-ethyl ester (21780-39-2) → 3-chlorophenylisocyanic acid (13400-54-9)

Guidance literature:

Kinetics; acid-catalyzed hydroylsis;

upstream raw materials:

(3-chloro-phenyl)-carbamic acid pyridin-2-ylmethyl ester

(3-Chloro-phenyl)-carbamic acid 2-pyridin-2-yl-ethyl ester

(3-Chloro-phenyl)-carbamic acid 2-thiophen-2-yl-ethyl ester

m-chlorophenyl isocyanate

Downstream raw materials:

2-[3-(3-chlorophenylcarbamoyloxymethyl)-4-ethoxybenzyl]-tetrahydro-2-furancarboxylic acid

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