N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine ethyl ester

Base Information

Chemical Name:N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine ethyl ester
CAS No.:136670-07-0
Molecular Formula:C₂₈H₃₂N₄O₃
Molecular Weight:472.587
Hs Code.:

Synonyms:N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine ethyl ester

Suppliers and Price of N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine ethyl ester

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Technology Process of N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine ethyl ester

There total 2 articles about N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5878-41-1
lysergamine

: 136670-07-0
N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / dimethylformamide / 3 h / Ambient temperature

2: 79 percent / KOH / ethanol / 3 h / Ambient temperature

3: 1) 1,1'-carbonyldiimidazole / 1) dioxane, reflux, 15 min, 2) dioxane, reflux, 3 h

With potassium hydroxide; 1,1'-carbonyldiimidazole; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0223-5234(99)80045-2

Reference yield:

: 229156-14-3
N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-iminodiacetic acid diethyl ester

: 136670-07-0
N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / KOH / ethanol / 3 h / Ambient temperature

2: 1) 1,1'-carbonyldiimidazole / 1) dioxane, reflux, 15 min, 2) dioxane, reflux, 3 h

With potassium hydroxide; 1,1'-carbonyldiimidazole; In ethanol;
DOI:10.1016/S0223-5234(99)80045-2