N,N-dimethyl-6-amino-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-D-glycero-α-D-gluco-heptofuranuronamide

Base Information

Chemical Name:N,N-dimethyl-6-amino-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-D-glycero-α-D-gluco-heptofuranuronamide
CAS No.:1017834-24-0
Molecular Formula:C₁₉H₂₈N₂O₆
Molecular Weight:380.441
Hs Code.:

Synonyms:N,N-dimethyl-6-amino-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-D-glycero-α-D-gluco-heptofuranuronamide

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Chemical Property of N,N-dimethyl-6-amino-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-D-glycero-α-D-gluco-heptofuranuronamide

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Technology Process of N,N-dimethyl-6-amino-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-D-glycero-α-D-gluco-heptofuranuronamide

There total 3 articles about N,N-dimethyl-6-amino-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-D-glycero-α-D-gluco-heptofuranuronamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1017834-20-6
C₁₉H₂₅NO₆

: 1017834-24-0
N,N-dimethyl-6-amino-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-D-glycero-α-D-gluco-heptofuranuronamide

Guidance literature:: With ammonium hydroxide; In water; at 20 ℃; for 48h; regioselective reaction; Sealed tube;
DOI:10.1016/j.tetasy.2012.12.005

Reference yield:

: 23558-05-6
3-O-benzyl-1,2-O-isopropylidene-1,5-D-xylo-dialdofuranose

: 1017834-24-0
N,N-dimethyl-6-amino-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-D-glycero-α-D-gluco-heptofuranuronamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / dichloromethane; water / 1 h / 20 °C

2: ammonium hydroxide / water / 48 h / 20 °C / Sealed tube

With ammonium hydroxide; sodium hydroxide; In dichloromethane; water;
DOI:10.1016/j.tetasy.2012.12.005

Reference yield:

: 22529-61-9
(1R)-1-((3aR,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro(2,3-d)(1,3)dioxol-5-yl)ethane-1,2-diol

: 1017834-24-0
N,N-dimethyl-6-amino-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-D-glycero-α-D-gluco-heptofuranuronamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium periodate; silica gel / dichloromethane

2: sodium hydroxide / dichloromethane; water / 1 h / 20 °C

3: ammonium hydroxide / water / 48 h / 20 °C / Sealed tube

With ammonium hydroxide; sodium periodate; silica gel; sodium hydroxide; In dichloromethane; water;
DOI:10.1016/j.tetasy.2012.12.005