Technology Process of C29H29N3O
There total 6 articles about C29H29N3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trimethylsilyl trifluoromethanesulfonate;
In
dichloromethane;
at 0 ℃;
for 3h;
Inert atmosphere;
DOI:10.3987/COM-13-12917
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diisobutylaluminium hydride / toluene / 0.75 h / -78 °C
2: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / 0 °C / Inert atmosphere
With
trimethylsilyl trifluoromethanesulfonate; diisobutylaluminium hydride;
In
dichloromethane; toluene;
DOI:10.3987/COM-13-12917
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 4 h / 20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / 0 °C
3: diisobutylaluminium hydride / toluene / 0.75 h / -78 °C
4: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / 0 °C / Inert atmosphere
With
dmap; lithium aluminium tetrahydride; trimethylsilyl trifluoromethanesulfonate; diisobutylaluminium hydride; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.3987/COM-13-12917