6-methyl-benzo[1,3]dioxole-5-sulfonic acid 2-hydrazinocarbonyl-phenyl ester

Base Information

• Chemical Name: 6-methyl-benzo[1,3]dioxole-5-sulfonic acid 2-hydrazinocarbonyl-phenyl ester
• CAS No.: 930088-10-1
• Molecular Formula: C₁₅H₁₄N₂O₆S
• Molecular Weight: 350.352

Synonyms:6-methyl-benzo[1,3]dioxole-5-sulfonic acid 2-hydrazinocarbonyl-phenyl ester

Chemical Property of 6-methyl-benzo[1,3]dioxole-5-sulfonic acid 2-hydrazinocarbonyl-phenyl ester

Chemical Property:

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Technology Process of 6-methyl-benzo[1,3]dioxole-5-sulfonic acid 2-hydrazinocarbonyl-phenyl ester

There total 1 articles about 6-methyl-benzo[1,3]dioxole-5-sulfonic acid 2-hydrazinocarbonyl-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2-(6-methyl-benzo[1,3]dioxole-5-sulfonyloxy)-benzoic acid methyl ester (930088-07-6) → 6-methyl-benzo[1,3]dioxole-5-sulfonic acid 2-hydrazinocarbonyl-phenyl ester (930088-10-1)

Guidance literature:

With hydrazine hydrate; In ethanol; at 20 ℃; for 2h;

DOI:10.1016/j.ejmech.2007.03.032

Reference yield: 89.0%

6-methyl-benzo[1,3]dioxole-5-sulfonic acid 2-hydrazinocarbonyl-phenyl ester (930088-10-1) + 4-Carboxybenzaldehyde (619-66-9) → 6-methyl-benzo[1,3]dioxole-5-sulfonic acid 2-(4-carboxy-benzylidene-hydrazinocarbonyl)-phenyl ester (1018788-12-9)

Guidance literature:

With hydrogenchloride; In ethanol; Heating;

DOI:10.1016/j.ejmech.2007.03.032

upstream raw materials:

2-(6-methyl-benzo[1,3]dioxole-5-sulfonyloxy)-benzoic acid methyl ester

Downstream raw materials:

6-methyl-benzo[1,3]dioxole-5-sulfonic acid 2-(4-carboxy-benzylidene-hydrazinocarbonyl)-phenyl ester

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