Technology Process of C17H15N3O3S2
There total 5 articles about C17H15N3O3S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: trifluoroacetic anhydride / phosphoric acid / 0.08 h / 20 °C
2.1: Oxone / methanol; tetrahydrofuran / 4 h / 20 °C
3.1: sodium methylate / methanol / 20 °C
3.2: 20 °C
4.1: hydrogenchloride / water / Reflux
With
hydrogenchloride; sodium methylate; trifluoroacetic anhydride;
In
tetrahydrofuran; methanol; phosphoric acid; water;
DOI:10.1016/j.bmc.2013.12.002
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium methylate / methanol / 20 °C
1.2: 20 °C
2.1: hydrogenchloride / water / Reflux
With
hydrogenchloride; sodium methylate;
In
methanol; water;
DOI:10.1016/j.bmc.2013.12.002
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: trifluoroacetic anhydride / phosphoric acid / 0.08 h / 20 °C
2.1: Oxone / methanol; tetrahydrofuran / 4 h / 20 °C
3.1: sodium methylate / methanol / 20 °C
3.2: 20 °C
4.1: hydrogenchloride / water / Reflux
With
hydrogenchloride; sodium methylate; trifluoroacetic anhydride;
In
tetrahydrofuran; methanol; phosphoric acid; water;
DOI:10.1016/j.bmc.2013.12.002