2-[3,3''-di(2-benzofuryl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine

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Chemical Name:2-[3,3''-di(2-benzofuryl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine
CAS No.:1268250-81-2
Molecular Formula:C₅₀H₃₂N₂O₂
Molecular Weight:692.816
Hs Code.:

Synonyms:2-[3,3''-di(2-benzofuryl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine

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Chemical Property of 2-[3,3''-di(2-benzofuryl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine

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Technology Process of 2-[3,3''-di(2-benzofuryl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine

There total 2 articles about 2-[3,3''-di(2-benzofuryl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 98437-24-2
benzofuran-2-boronic acid

: 1268250-80-1
2-(3,3''-dichloro-(1,1':3',1''-terphenyl-5'-yl))-4,6-diphenylpyrimidine

: 1268250-81-2
2-[3,3''-di(2-benzofuryl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine

Guidance literature:: With caesium carbonate; XPhos; palladium diacetate; In 1,4-dioxane; for 14h; Inert atmosphere; Reflux;

Reference yield:

: 942132-67-4
2-(3,5-dibromophenyl)-4,6-diphenylpyrimidine

: 63503-60-6
3-chlorophenylboronic acid

: 1268250-81-2
2-[3,3''-di(2-benzofuryl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 15 h / Inert atmosphere; Reflux

2: caesium carbonate; XPhos / palladium diacetate / 1,4-dioxane / 14 h / Inert atmosphere; Reflux

With caesium carbonate; XPhos; bis-triphenylphosphine-palladium(II) chloride; palladium diacetate; In tetrahydrofuran; 1,4-dioxane;