4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1',1'',1'''-tetraoxide

Base Information

Chemical Name:4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1',1'',1'''-tetraoxide
CAS No.:459425-54-8
Molecular Formula:C₃₂H₂₂N₄O₄
Molecular Weight:526.551
Hs Code.:

Synonyms:4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1',1'',1'''-tetraoxide

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Chemical Property of 4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1',1'',1'''-tetraoxide

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Technology Process of 4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1',1'',1'''-tetraoxide

There total 1 articles about 4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1',1'',1'''-tetraoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 158982-94-6
4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine

: 459425-54-8
4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1',1'',1'''-tetraoxide

Guidance literature:: With dihydrogen peroxide; urea; trifluoroacetic anhydride; In acetonitrile; at 50 ℃; for 48h;
DOI:10.1039/b203087j

Reference yield: 76.0%

: gadolinium(III) perchlorate

: 459425-54-8
4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1',1'',1'''-tetraoxide

: [Gd(4',4''-diphenyl-2,2':6',2'':6'',2''-quaterpyridine-1,1',1'',1'''-O₄)2][ClO₄]3

Guidance literature:: In ethanol; metal perchlorate salt was dissolved in min amount of ethanol and added to a suspn. of ligand in hot ethanol; ppt. was filtered, recrystd. by vapor diffusion of diethyl ether into a CH3CN soln.; elem. anal.;
DOI:10.1039/b203087j