2-benzyl-5-hydroxy-6-methylpyridine-3,4-dicarboxylic acid dimethyl ester

Base Information

Chemical Name:2-benzyl-5-hydroxy-6-methylpyridine-3,4-dicarboxylic acid dimethyl ester
CAS No.:1345962-81-3
Molecular Formula:C₁₇H₁₇NO₅
Molecular Weight:315.326
Hs Code.:

Synonyms:2-benzyl-5-hydroxy-6-methylpyridine-3,4-dicarboxylic acid dimethyl ester

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Chemical Property of 2-benzyl-5-hydroxy-6-methylpyridine-3,4-dicarboxylic acid dimethyl ester

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Technology Process of 2-benzyl-5-hydroxy-6-methylpyridine-3,4-dicarboxylic acid dimethyl ester

There total 6 articles about 2-benzyl-5-hydroxy-6-methylpyridine-3,4-dicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.1%

: 68484-91-3
2-benzyl-4-methyl-5-ethoxy-1,3-oxazole

: 624-48-6
dimethyl cis-but-2-ene-1,4-dioate

: 1345962-81-3
2-benzyl-5-hydroxy-6-methylpyridine-3,4-dicarboxylic acid dimethyl ester

Guidance literature:: for 5h; Reflux;

Reference yield:

: C₁₉H₂₁NO₅

: 1345962-81-3
2-benzyl-5-hydroxy-6-methylpyridine-3,4-dicarboxylic acid dimethyl ester

Guidance literature:: With hydrogenchloride; water; In ethanol;
DOI:10.1016/j.ejmech.2013.10.026

Reference yield:

: 103-82-2
phenylacetic acid

: 1345962-81-3
2-benzyl-5-hydroxy-6-methylpyridine-3,4-dicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 12.5 h / 20 °C

2: phosphorus pentoxide / chloroform / 4 h / Reflux

3: 5 h / Reflux

With phosphorus pentoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; chloroform;