3-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-5-phenyl-3H-[1,3,4]oxadiazole-2-thione

Base Information

Chemical Name:3-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-5-phenyl-3H-[1,3,4]oxadiazole-2-thione
CAS No.:394692-96-7
Molecular Formula:C₁₃H₁₄N₂O₅S
Molecular Weight:310.331
Hs Code.:

Synonyms:3-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-5-phenyl-3H-[1,3,4]oxadiazole-2-thione

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Chemical Property of 3-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-5-phenyl-3H-[1,3,4]oxadiazole-2-thione

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Technology Process of 3-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-5-phenyl-3H-[1,3,4]oxadiazole-2-thione

There total 4 articles about 3-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-5-phenyl-3H-[1,3,4]oxadiazole-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 394692-95-6
C₃₄H₂₆N₂O₈S

: 394692-96-7
3-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-5-phenyl-3H-[1,3,4]oxadiazole-2-thione

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 48h;

Reference yield:

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 394692-96-7
3-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-5-phenyl-3H-[1,3,4]oxadiazole-2-thione

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 24 h / 20 °C

2: 55 percent / NaOCH₃ / methanol / 48 h / 20 °C

With trimethylsilyl trifluoromethanesulfonate; sodium methylate; In methanol; 1,2-dichloro-ethane;

Reference yield:

: 3004-42-0
5-phenyl-1,3,4-oxadiazole-2(3H)-thione

: 394692-96-7
3-((2R,3R,4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-5-phenyl-3H-[1,3,4]oxadiazole-2-thione

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium sulfate / 10 h / Heating

2: trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 24 h / 20 °C

3: 55 percent / NaOCH₃ / methanol / 48 h / 20 °C

With ammonium sulfate; trimethylsilyl trifluoromethanesulfonate; sodium methylate; In methanol; 1,2-dichloro-ethane;