2-(bromomethyl)-6-methyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydroquinoline

Base Information

Chemical Name:2-(bromomethyl)-6-methyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydroquinoline
CAS No.:1269261-67-7
Molecular Formula:C₁₈H₂₀BrNO₂S
Molecular Weight:394.332
Hs Code.:

Synonyms:2-(bromomethyl)-6-methyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydroquinoline

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Chemical Property of 2-(bromomethyl)-6-methyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydroquinoline

Chemical Property:

Purity/Quality:

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Technology Process of 2-(bromomethyl)-6-methyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydroquinoline

There total 10 articles about 2-(bromomethyl)-6-methyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1269261-49-5
N-(2-(but-3-en-1-yl)-4-methylphenyl)-4-methylbenzenesulfonamide

: 1269261-67-7
2-(bromomethyl)-6-methyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydroquinoline

Guidance literature:: With palladium diacetate; potassium carbonate; copper(ll) bromide; In tetrahydrofuran; at 25 ℃; for 72h; Inert atmosphere;
DOI:10.1016/j.tet.2010.12.017

Reference yield:

: 1269261-49-5
N-(2-(but-3-en-1-yl)-4-methylphenyl)-4-methylbenzenesulfonamide

: 1269261-67-7
2-(bromomethyl)-6-methyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydroquinoline

: 1269261-81-5
N-[2-(3,4-dibromobutyl)-4-methylphenyl]-4-methylbenzenesulfonamide

Guidance literature:: With palladium diacetate; potassium carbonate; copper(ll) bromide; In acetonitrile; at 25 ℃; for 72h; Inert atmosphere;
DOI:10.1016/j.tet.2010.12.017

Reference yield:

: 895578-39-9
N-(2-(chloromethyl)-4-methylphenyl)-4-methylbenzenesulfonamide

: 1269261-67-7
2-(bromomethyl)-6-methyl-1-(toluene-4-sulfonyl)-1,2,3,4-tetrahydroquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

2: palladium diacetate; potassium carbonate; copper(ll) bromide / tetrahydrofuran / 72 h / 25 °C / Inert atmosphere

With palladium diacetate; potassium carbonate; copper(ll) bromide; In tetrahydrofuran;
DOI:10.1016/j.tet.2010.12.017