[1-(6-tert-butyl-pyridin-2-yl)-ethylidene]-(2,6-diisopropyl-phenyl)-amine

Base Information

Chemical Name:[1-(6-tert-butyl-pyridin-2-yl)-ethylidene]-(2,6-diisopropyl-phenyl)-amine
CAS No.:900816-57-1
Molecular Formula:C₂₃H₃₂N₂
Molecular Weight:336.52
Hs Code.:

[1-(6-<i>tert</i>-butyl-pyridin-2-yl)-ethylidene]-(2,6-diisopropyl-phenyl)-amine

Synonyms:[1-(6-tert-butyl-pyridin-2-yl)-ethylidene]-(2,6-diisopropyl-phenyl)-amine

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Chemical Property of [1-(6-tert-butyl-pyridin-2-yl)-ethylidene]-(2,6-diisopropyl-phenyl)-amine

Chemical Property:

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Technology Process of [1-(6-tert-butyl-pyridin-2-yl)-ethylidene]-(2,6-diisopropyl-phenyl)-amine

There total 6 articles about [1-(6-tert-butyl-pyridin-2-yl)-ethylidene]-(2,6-diisopropyl-phenyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 900816-51-5
1-(6-(tert-butyl)pyridin-2-yl)ethan-1-one

: 24544-04-5
2,6-diisopropylbenzenamine

: 900816-57-1
[1-(6-tert-butyl-pyridin-2-yl)-ethylidene]-(2,6-diisopropyl-phenyl)-amine

Guidance literature:: With formic acid; In methanol; at 65 ℃;
DOI:10.1002/ejic.200500645

Reference yield:

: 100-71-0
2-Ethylpyridine

: 900816-57-1
[1-(6-tert-butyl-pyridin-2-yl)-ethylidene]-(2,6-diisopropyl-phenyl)-amine

Guidance literature:: Multi-step reaction with 6 steps

1.1: nBuLi / -30 °C

1.2: 67 percent / -50 °C

2.1: KN(iPr)2 / -50 °C

2.2: 68 percent / -75 °C

3.1: 79 percent / m-chloroperbenzoic acid / CHCl₃ / 0 °C

4.1: 65 percent / dimethylcarbamoyl chloride / CH₂Cl₂

5.1: diethyl ether / -25 °C

5.2: 36 percent / H₂O; NH₃Cl; HCl

6.1: 85 percent / formic acid / methanol / 65 °C

With n-butyllithium; formic acid; potassium diisopropyl amide; 3-chloro-benzenecarboperoxoic acid; N,N-Dimethylcarbamoyl chloride; In methanol; diethyl ether; dichloromethane; chloroform;
DOI:10.1002/ejic.200500645

Reference yield:

: 5944-41-2
2-tert-butylpyridine

: 900816-57-1
[1-(6-tert-butyl-pyridin-2-yl)-ethylidene]-(2,6-diisopropyl-phenyl)-amine

Guidance literature:: Multi-step reaction with 4 steps

1.1: 79 percent / m-chloroperbenzoic acid / CHCl₃ / 0 °C

2.1: 65 percent / dimethylcarbamoyl chloride / CH₂Cl₂

3.1: diethyl ether / -25 °C

3.2: 36 percent / H₂O; NH₃Cl; HCl

4.1: 85 percent / formic acid / methanol / 65 °C

With formic acid; 3-chloro-benzenecarboperoxoic acid; N,N-Dimethylcarbamoyl chloride; In methanol; diethyl ether; dichloromethane; chloroform;
DOI:10.1002/ejic.200500645