6-benzhydrylidene-13-[bis-(4-dodecyloxy-phenyl)-methylene]-6,13-dihydro-pentacene

Base Information

Chemical Name:6-benzhydrylidene-13-[bis-(4-dodecyloxy-phenyl)-methylene]-6,13-dihydro-pentacene
CAS No.:954097-68-8
Molecular Formula:C₇₂H₈₀O₂
Molecular Weight:977.426
Hs Code.:

Synonyms:6-benzhydrylidene-13-[bis-(4-dodecyloxy-phenyl)-methylene]-6,13-dihydro-pentacene

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Chemical Property of 6-benzhydrylidene-13-[bis-(4-dodecyloxy-phenyl)-methylene]-6,13-dihydro-pentacene

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Technology Process of 6-benzhydrylidene-13-[bis-(4-dodecyloxy-phenyl)-methylene]-6,13-dihydro-pentacene

There total 11 articles about 6-benzhydrylidene-13-[bis-(4-dodecyloxy-phenyl)-methylene]-6,13-dihydro-pentacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: C₇₂H₈₀O₂S

: 954097-68-8
6-benzhydrylidene-13-[bis-(4-dodecyloxy-phenyl)-methylene]-6,13-dihydro-pentacene

Guidance literature:: With triphenylphosphine; In xylene; for 10h; Heating;
DOI:10.1002/anie.200502142

Reference yield:

: 879219-96-2
pentacen-6(13H)-thione

: 954097-68-8
6-benzhydrylidene-13-[bis-(4-dodecyloxy-phenyl)-methylene]-6,13-dihydro-pentacene

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / tetrahydrofuran / 1 h

2: 92 percent / PPh₃ / xylene / 12 h / Heating

3: 56.7 percent / KMnO₄ / acetone / 2 h / 20 °C

4: 98 percent / Lawesson reagent / toluene / 0.5 h / 80 °C

5: 88 percent / tetrahydrofuran / 1 h

6: 87 percent / PPh₃ / xylene / 10 h / Heating

With Lawessons reagent; potassium permanganate; triphenylphosphine; In tetrahydrofuran; acetone; toluene; xylene;
DOI:10.1002/anie.200502142

Reference yield:

: 954097-63-3
6-benzhydrylidene-6,13-dihydro-pentacene

: 954097-68-8
6-benzhydrylidene-13-[bis-(4-dodecyloxy-phenyl)-methylene]-6,13-dihydro-pentacene

Guidance literature:: Multi-step reaction with 4 steps

1: 56.7 percent / KMnO₄ / acetone / 2 h / 20 °C

2: 98 percent / Lawesson reagent / toluene / 0.5 h / 80 °C

3: 88 percent / tetrahydrofuran / 1 h

4: 87 percent / PPh₃ / xylene / 10 h / Heating

With Lawessons reagent; potassium permanganate; triphenylphosphine; In tetrahydrofuran; acetone; toluene; xylene;
DOI:10.1002/anie.200502142