N⁶-Benzoyl-3'-O-(tert-butyldimethylsilyl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N⁶,N⁶,2'-O,3'-O-tetrabenzoyladenosin

Base Information

• Chemical Name: N⁶-Benzoyl-3'-O-(tert-butyldimethylsilyl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N⁶,N⁶,2'-O,3'-O-tetrabenzoyladenosin
• CAS No.: 80727-14-6
• Molecular Formula: C₆₇H₆₂ClN₁₀O₁₅PSi
• Molecular Weight: 1341.8

Synonyms:N⁶-Benzoyl-3'-O-(tert-butyldimethylsilyl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N⁶,N⁶,2'-O,3'-O-tetrabenzoyladenosin

Chemical Property of N⁶-Benzoyl-3'-O-(tert-butyldimethylsilyl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N⁶,N⁶,2'-O,3'-O-tetrabenzoyladenosin

Chemical Property:

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Technology Process of N⁶-Benzoyl-3'-O-(tert-butyldimethylsilyl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N⁶,N⁶,2'-O,3'-O-tetrabenzoyladenosin

There total 1 articles about N⁶-Benzoyl-3'-O-(tert-butyldimethylsilyl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N⁶,N⁶,2'-O,3'-O-tetrabenzoyladenosin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

N6-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl-<2'-P-(2-chlorphenyl)>-5'>-N6,N6,2'-O,3'-O-tetrabenzoyladenosin (80727-13-5) → N6-Benzoyl-3'-O-(tert-butyldimethylsilyl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N6,N6,2'-O,3'-O-tetrabenzoyladenosin (80727-14-6)

Guidance literature:

With trifluoric acid; In chloroform; for 0.666667h; Ambient temperature;

Reference yield:

N6-Benzoyl-3'-O-(tert-butyldimethylsilyl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N6,N6,2'-O,3'-O-tetrabenzoyladenosin (80727-14-6) + Triethylammonium-6-benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenosin-2'-(2-chlorphenyl)phosphat> (75082-94-9) → N6-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N6-benzoyl-3'-O-(tert-butyldimetylsilyl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N6,N6,2'-O,3'-O-tetrabenzoyladenosin (75085-70-0)

Guidance literature:

Yield given. Multistep reaction;

upstream raw materials:

N⁶-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl-<2'-P-(2-chlorphenyl)>-5'>-N⁶,N⁶,2'-O,3'-O-tetrabenzoyladenosin

Downstream raw materials:

N⁶-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-3'-O-(tert-butyldimetylsilyl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N⁶,N⁶,2'-O,3'-O-tetrabenzoyladenosin

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