2-(2,8-dimethyl-11,12-dihydro-6H-dibenzo[b,f][1,5]diazocin-5-yl)-1-phenyl-ethanone

Base Information

• Chemical Name: 2-(2,8-dimethyl-11,12-dihydro-6H-dibenzo[b,f][1,5]diazocin-5-yl)-1-phenyl-ethanone
• CAS No.: 1225379-24-7
• Molecular Formula: C₂₄H₂₄N₂O
• Molecular Weight: 356.467

Synonyms:2-(2,8-dimethyl-11,12-dihydro-6H-dibenzo[b,f][1,5]diazocin-5-yl)-1-phenyl-ethanone

Chemical Property of 2-(2,8-dimethyl-11,12-dihydro-6H-dibenzo[b,f][1,5]diazocin-5-yl)-1-phenyl-ethanone

Chemical Property:

Purity/Quality:

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Technology Process of 2-(2,8-dimethyl-11,12-dihydro-6H-dibenzo[b,f][1,5]diazocin-5-yl)-1-phenyl-ethanone

There total 2 articles about 2-(2,8-dimethyl-11,12-dihydro-6H-dibenzo[b,f][1,5]diazocin-5-yl)-1-phenyl-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(+/-)-2,8-dimethyl-5-(2-oxo-2-phenyl-ethyl)-6H,12H-5,11-methano-dibenzo[b,f][1,5]diazocin-5-ium bromide (1190482-38-2) → 2-(2,8-dimethyl-11,12-dihydro-6H-dibenzo[b,f][1,5]diazocin-5-yl)-1-phenyl-ethanone (1225379-24-7) + (+/-)-2,8-dimethyl-6H,12H-5,11-[benzoyl-ethano]-dibenzo[b,f][1,5]diazocine

Guidance literature:

With aluminum oxide; In chloroform; at 25 ℃; for 2.5h; diastereoselective reaction; Inert atmosphere;

DOI:10.1039/b925065d

Reference yield:

(+/-)-2,8-dimethyl-5-(2-oxo-2-phenyl-ethyl)-6H,12H-5,11-methano-dibenzo[b,f][1,5]diazocin-5-ium bromide (1190482-38-2) → 2-(2,8-dimethyl-11,12-dihydro-6H-dibenzo[b,f][1,5]diazocin-5-yl)-1-phenyl-ethanone (1225379-24-7)

Guidance literature:

With sodium hydroxide;

DOI:10.1039/b925065d

upstream raw materials:

(+/-)-2,8-dimethyl-5-(2-oxo-2-phenyl-ethyl)-6H,12H-5,11-methano-dibenzo[b,f][1,5]diazocin-5-ium bromide

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