Technology Process of C61H79N2O16PSi
There total 6 articles about C61H79N2O16PSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tert.-butylhydroperoxide;
In
dichloromethane;
at -50 ℃;
for 1h;
DOI:10.1021/ol201806d
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium tetrahydroborate / tetrahydrofuran; 2-methyl-propan-1-ol; water / 0 - 20 °C
2.1: acetic acid / tetrahydrofuran; 2-methyl-propan-1-ol; water / 0 °C / Heating
2.2: 0.5 h / 20 °C
2.3: 3 h
3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C
3.2: 2 h / 0 °C
4.1: N-iodo-succinimide; water / acetone / 0 - 20 °C
5.1: 1H-tetrazole / dichloromethane / 0 - 20 °C
6.1: tert.-butylhydroperoxide / dichloromethane / 1 h / -50 °C
With
1H-tetrazole; tert.-butylhydroperoxide; sodium tetrahydroborate; N-iodo-succinimide; water; sodium hydride; acetic acid;
In
tetrahydrofuran; dichloromethane; 2-methyl-propan-1-ol; water; acetone; mineral oil;
DOI:10.1021/ol201806d
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C
1.2: 2 h / 0 °C
2.1: N-iodo-succinimide; water / acetone / 0 - 20 °C
3.1: 1H-tetrazole / dichloromethane / 0 - 20 °C
4.1: tert.-butylhydroperoxide / dichloromethane / 1 h / -50 °C
With
1H-tetrazole; tert.-butylhydroperoxide; N-iodo-succinimide; water; sodium hydride;
In
tetrahydrofuran; dichloromethane; acetone; mineral oil;
DOI:10.1021/ol201806d
