(Z)-isoc-11-enal

Base Information

Chemical Name:(Z)-isoc-11-enal
CAS No.:123134-08-7
Molecular Formula:C₂₀H₃₈O
Molecular Weight:294.521
Hs Code.:

Synonyms:(Z)-isoc-11-enal

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Chemical Property of (Z)-isoc-11-enal

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Technology Process of (Z)-isoc-11-enal

There total 1 articles about (Z)-isoc-11-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2423-10-1
Oleic aldehyde

: 123134-08-7
(Z)-isoc-11-enal

Guidance literature:: Multi-step reaction with 6 steps

1: 87.5 percent / p-toluenesulfonic acid / benzene / 20 h / Heating

2: 1.) 9-BBN / 1.) THF, 25 deg C, 3 h, 2.) methanol, reflux, 2 h

3: 1.) 9-BBN, 2.) lithium diisopropylamide, 3.) NaOH, H₂O₂

4: diethyl ether

5: 70 percent / LAH / diethyl ether / 5 h

6: 91 percent / pyridinium chlorochromate / CH₂Cl₂ / 1 h

With sodium hydroxide; lithium aluminium tetrahydride; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; toluene-4-sulfonic acid; pyridinium chlorochromate; lithium diisopropyl amide; In diethyl ether; dichloromethane; benzene;

Reference yield:

: 123134-08-7
(Z)-isoc-11-enal

: 27519-02-4
(Z)-tricos-9-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / diethyl ether / 5 h / Heating

2: 96 percent / pyridine / 24 h / Heating

3: 95 percent / LAH / diethyl ether

With pyridine; lithium aluminium tetrahydride; In diethyl ether;

Reference yield:

: 123134-08-7
(Z)-isoc-11-enal

: (S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (Z)-(R)-1-trimethylsilanylethynyl-icos-11-enyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -12 °C

1.2: 76 percent / tetrahydrofuran; hexane / 1.5 h / -12 °C

2.1: 93 percent / o-iodoxybenzoic acid / dimethylsulfoxide; tetrahydrofuran / 3 h / 20 °C

3.1: chiral ruthenium catalyst / propan-2-ol / 30 °C

4.1: oxalyl chloride; DMF / hexane / 2 h / 20 °C

With n-butyllithium; oxalyl dichloride; N,N-dimethyl-formamide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; chiral ruthenium catalyst; In tetrahydrofuran; hexane; dimethyl sulfoxide; isopropyl alcohol; 3.1: Noyori asymmetric reduction;
DOI:10.1016/j.tet.2005.05.034