N₁,N₅,N₁₀,N₁₄-tertakis[3-(4-acetoxyphenyl)-2-methyl-2-propenoyl]-1,5,10,14-tetraazatetradecane

Base Information

• Chemical Name: N₁,N₅,N₁₀,N₁₄-tertakis[3-(4-acetoxyphenyl)-2-methyl-2-propenoyl]-1,5,10,14-tetraazatetradecane
• CAS No.: 402598-61-2
• Molecular Formula: C₅₈H₆₆N₄O₁₂
• Molecular Weight: 1011.18

Synonyms:N₁,N₅,N₁₀,N₁₄-tertakis[3-(4-acetoxyphenyl)-2-methyl-2-propenoyl]-1,5,10,14-tetraazatetradecane

Chemical Property of N₁,N₅,N₁₀,N₁₄-tertakis[3-(4-acetoxyphenyl)-2-methyl-2-propenoyl]-1,5,10,14-tetraazatetradecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N₁,N₅,N₁₀,N₁₄-tertakis[3-(4-acetoxyphenyl)-2-methyl-2-propenoyl]-1,5,10,14-tetraazatetradecane

There total 4 articles about N₁,N₅,N₁₀,N₁₄-tertakis[3-(4-acetoxyphenyl)-2-methyl-2-propenoyl]-1,5,10,14-tetraazatetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

Spermine (71-44-3) + (E)-3-(4-hydroxyphenyl)-2-methyl-2-propenoyl chloride (402598-52-1) → N1,N5,N10,N14-tertakis[3-(4-acetoxyphenyl)-2-methyl-2-propenoyl]-1,5,10,14-tetraazatetradecane (402598-61-2)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃;

DOI:10.1248/cpb.50.47

Reference yield:

(E)-3-(4-hydroxyphenyl)-2-methyl-prop-2-enoic acid (113277-24-0,5325-37-1) → N1,N5,N10,N14-tertakis[3-(4-acetoxyphenyl)-2-methyl-2-propenoyl]-1,5,10,14-tetraazatetradecane (402598-61-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 70 percent / pyridine / 5 h / 20 °C

2: thionyl chloride / CH₂Cl₂ / 24 h / 20 °C

3: 98 percent / Et₃N / tetrahydrofuran / 20 °C

With pyridine; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1248/cpb.50.47

Reference yield:

4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → N1,N5,N10,N14-tertakis[3-(4-acetoxyphenyl)-2-methyl-2-propenoyl]-1,5,10,14-tetraazatetradecane (402598-61-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 27 percent / piperidine; pyridine / 25 h / 100 °C

2: 70 percent / pyridine / 5 h / 20 °C

3: thionyl chloride / CH₂Cl₂ / 24 h / 20 °C

4: 98 percent / Et₃N / tetrahydrofuran / 20 °C

With piperidine; pyridine; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1248/cpb.50.47

upstream raw materials:

Spermine

(E)-3-(4-hydroxyphenyl)-2-methyl-2-propenoyl chloride

(E)-3-(4-hydroxyphenyl)-2-methyl-prop-2-enoic acid

4-hydroxy-benzaldehyde

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 402598-61-2 N₁,N₅,N₁₀,N₁₄-tertakis[3-(4-acetoxyphenyl)-2-methyl-2-propenoyl]-1,5,10,14-tetraazatetradecane

Send

Send

Metric Ton KG G Pound L ML

Send

Send