2-((2S,3R,4S,5R,6S)-3-Azido-4,5-bis-benzyloxy-6-methoxy-tetrahydro-pyran-2-yl)-1,3-diphenyl-imidazolidine

Base Information

Chemical Name:2-((2S,3R,4S,5R,6S)-3-Azido-4,5-bis-benzyloxy-6-methoxy-tetrahydro-pyran-2-yl)-1,3-diphenyl-imidazolidine
CAS No.:74844-35-2
Molecular Formula:C₃₅H₃₇N₅O₄
Molecular Weight:591.71
Hs Code.:

Synonyms:2-((2S,3R,4S,5R,6S)-3-Azido-4,5-bis-benzyloxy-6-methoxy-tetrahydro-pyran-2-yl)-1,3-diphenyl-imidazolidine

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Chemical Property of 2-((2S,3R,4S,5R,6S)-3-Azido-4,5-bis-benzyloxy-6-methoxy-tetrahydro-pyran-2-yl)-1,3-diphenyl-imidazolidine

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Technology Process of 2-((2S,3R,4S,5R,6S)-3-Azido-4,5-bis-benzyloxy-6-methoxy-tetrahydro-pyran-2-yl)-1,3-diphenyl-imidazolidine

There total 4 articles about 2-((2S,3R,4S,5R,6S)-3-Azido-4,5-bis-benzyloxy-6-methoxy-tetrahydro-pyran-2-yl)-1,3-diphenyl-imidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29388-46-3
methyl 2,3-di-O-benzyl-α-D-galactopyranoside

: 74844-35-2
2-((2S,3R,4S,5R,6S)-3-Azido-4,5-bis-benzyloxy-6-methoxy-tetrahydro-pyran-2-yl)-1,3-diphenyl-imidazolidine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Pyridine, 75 deg C, 18 h; 2.) 0 deg C to room temperature, 2 days

2: 4:1 acetic acid, water / 4 h / 100 °C

3: 92 percent / sodium azide / dimethylformamide / 5 h / 120 °C

4: dicyclohexylcarbodiimide / 1.) DMSO, oxidation; 2.) methanol, room temp., 24 h

With sodium azide; water; acetic acid; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1021/jo01310a060

Reference yield:

: 71756-39-3
methyl 2,3-di-O-benzyl-4-O-mesyl-6-O-trityl-α-D-galactopyranoside

: 74844-35-2
2-((2S,3R,4S,5R,6S)-3-Azido-4,5-bis-benzyloxy-6-methoxy-tetrahydro-pyran-2-yl)-1,3-diphenyl-imidazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 4:1 acetic acid, water / 4 h / 100 °C

2: 92 percent / sodium azide / dimethylformamide / 5 h / 120 °C

3: dicyclohexylcarbodiimide / 1.) DMSO, oxidation; 2.) methanol, room temp., 24 h

With sodium azide; water; acetic acid; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1021/jo01310a060

Reference yield:

: 74844-34-1
Methanesulfonic acid (2R,3S,4R,5R,6S)-4,5-bis-benzyloxy-2-hydroxymethyl-6-methoxy-tetrahydro-pyran-3-yl ester

: 74844-35-2
2-((2S,3R,4S,5R,6S)-3-Azido-4,5-bis-benzyloxy-6-methoxy-tetrahydro-pyran-2-yl)-1,3-diphenyl-imidazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / sodium azide / dimethylformamide / 5 h / 120 °C

2: dicyclohexylcarbodiimide / 1.) DMSO, oxidation; 2.) methanol, room temp., 24 h

With sodium azide; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1021/jo01310a060