1-[O-2-(2-(E)-{4-[2-(E)-(2-hydroxyphenyl)vinyl]phenyl}vinyl)phenyl]-4-[O-2-(2-(E)-{4-[2-(E)-(2-benzyloxyphenyl)vinyl]phenyl}vnyl)phenyl]-2,3-[O-isopropylidene]-L-threitol

Base Information

• Chemical Name: 1-[O-2-(2-(E)-{4-[2-(E)-(2-hydroxyphenyl)vinyl]phenyl}vinyl)phenyl]-4-[O-2-(2-(E)-{4-[2-(E)-(2-benzyloxyphenyl)vinyl]phenyl}vnyl)phenyl]-2,3-[O-isopropylidene]-L-threitol
• CAS No.: 1214920-16-7
• Molecular Formula: C₅₈H₅₂O₆
• Molecular Weight: 845.047

Synonyms:1-[O-2-(2-(E)-{4-[2-(E)-(2-hydroxyphenyl)vinyl]phenyl}vinyl)phenyl]-4-[O-2-(2-(E)-{4-[2-(E)-(2-benzyloxyphenyl)vinyl]phenyl}vnyl)phenyl]-2,3-[O-isopropylidene]-L-threitol

Chemical Property of 1-[O-2-(2-(E)-{4-[2-(E)-(2-hydroxyphenyl)vinyl]phenyl}vinyl)phenyl]-4-[O-2-(2-(E)-{4-[2-(E)-(2-benzyloxyphenyl)vinyl]phenyl}vnyl)phenyl]-2,3-[O-isopropylidene]-L-threitol

Chemical Property:

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Technology Process of 1-[O-2-(2-(E)-{4-[2-(E)-(2-hydroxyphenyl)vinyl]phenyl}vinyl)phenyl]-4-[O-2-(2-(E)-{4-[2-(E)-(2-benzyloxyphenyl)vinyl]phenyl}vnyl)phenyl]-2,3-[O-isopropylidene]-L-threitol

There total 1 articles about 1-[O-2-(2-(E)-{4-[2-(E)-(2-hydroxyphenyl)vinyl]phenyl}vinyl)phenyl]-4-[O-2-(2-(E)-{4-[2-(E)-(2-benzyloxyphenyl)vinyl]phenyl}vnyl)phenyl]-2,3-[O-isopropylidene]-L-threitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

(E,E)-1,4-bis(2'-hydroxystyryl)benzene (65614-65-5) + p-toluenesulfonyl-4-O-{(2-(E)-{4-[2-(2-benzyloxyphenyl)-(E)-vinyl]phenyl}vinyl)phenyl}-2,3-O-isopropylidene-L-threitol (1214920-15-6) → 1-[O-2-(2-(E)-{4-[2-(E)-(2-hydroxyphenyl)vinyl]phenyl}vinyl)phenyl]-4-[O-2-(2-(E)-{4-[2-(E)-(2-benzyloxyphenyl)vinyl]phenyl}vnyl)phenyl]-2,3-[O-isopropylidene]-L-threitol (1214920-16-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 19h; Inert atmosphere;

DOI:10.1021/jp909286t

Reference yield: 63.0%

1-[O-2-(2-(E)-{4-[2-(E)-(2-hydroxyphenyl)vinyl]phenyl}vinyl)phenyl]-4-[O-2-(2-(E)-{4-[2-(E)-(2-benzyloxyphenyl)vinyl]phenyl}vnyl)phenyl]-2,3-[O-isopropylidene]-L-threitol (1214920-16-7) + (4S,5S)-4-hydroxymethyl-2,2-dimethyl-5-tosyloxymethyl-1,3-dioxolane (70831-49-1,73711-65-6,58789-44-9) → C65H64O9 (1214920-23-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 42h; Inert atmosphere;

DOI:10.1021/jp909286t

Reference yield: 31.0%

1-[O-2-(2-(E)-{4-[2-(E)-(2-hydroxyphenyl)vinyl]phenyl}vinyl)phenyl]-4-[O-2-(2-(E)-{4-[2-(E)-(2-benzyloxyphenyl)vinyl]phenyl}vnyl)phenyl]-2,3-[O-isopropylidene]-L-threitol (1214920-16-7) + (4S,5S)-2,2-dimethyl-4,5-bis(p-toluenesulfonyloxymethyl)-1,3-dioxolan (37002-45-2) → C123H114O14 (1214920-05-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 48h; Inert atmosphere;

DOI:10.1021/jp909286t

upstream raw materials:

(E,E)-1,4-bis(2'-hydroxystyryl)benzene

p-toluenesulfonyl-4-O-{(2-(E)-{4-[2-(2-benzyloxyphenyl)-(E)-vinyl]phenyl}vinyl)phenyl}-2,3-O-isopropylidene-L-threitol

Downstream raw materials:

C₆₅H₆₄O₉

C₁₂₃H₁₁₄O₁₄

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