N-(5-bromo-2-nitrophenyl)-1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinamine

Base Information

• Chemical Name: N-(5-bromo-2-nitrophenyl)-1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinamine
• CAS No.: 950772-30-2
• Molecular Formula: C₁₉H₂₈BrN₃O₃
• Molecular Weight: 426.354

Synonyms:N-(5-bromo-2-nitrophenyl)-1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinamine

Chemical Property of N-(5-bromo-2-nitrophenyl)-1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinamine

Chemical Property:

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Technology Process of N-(5-bromo-2-nitrophenyl)-1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinamine

There total 1 articles about N-(5-bromo-2-nitrophenyl)-1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-[trans-4-(ethoxy)cyclohexyl]-4-piperidinamine dihydrochloride + 4-bromo-2-fluoronitrobenzene (321-23-3) → N-(5-bromo-2-nitrophenyl)-1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinamine (950772-30-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 80 ℃;

Reference yield: 99.0%

N-(5-bromo-2-nitrophenyl)-1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinamine (950772-30-2) → 4-bromo-N2-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-1,2-benzenediamine (950772-31-3)

Guidance literature:

With hydrazine; nickel; In ethanol; at 20 ℃; for 3h;

Reference yield: 99.0%

N-(5-bromo-2-nitrophenyl)-1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinamine (950772-30-2) + tri-n-butyl(vinyl)tin (7486-35-3) → N-(5-ethenyl-2-nitrophenyl)-1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinamine (950772-32-4)

Guidance literature:

With triphenylphosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In toluene; at 20 - 120 ℃;

upstream raw materials:

4-bromo-2-fluoronitrobenzene

Downstream raw materials:

4-bromo-N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-1,2-benzenediamine

N-(5-ethenyl-2-nitrophenyl)-1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinamine

6-bromo-1-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-1,3-dihydro-2H-benzimidazol-2-one

4-ethyl-N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-1,2-benzenediamine

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