7-benzyl-4H-imidazo[1,5-d]thieno[2,3-b][1,4]thiazine-3-carboxylic acid

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Chemical Name:7-benzyl-4H-imidazo[1,5-d]thieno[2,3-b][1,4]thiazine-3-carboxylic acid
CAS No.:479638-73-8
Molecular Formula:C₁₆H₁₂N₂O₂S₂
Molecular Weight:328.415
Hs Code.:

Synonyms:7-benzyl-4H-imidazo[1,5-d]thieno[2,3-b][1,4]thiazine-3-carboxylic acid

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Chemical Property of 7-benzyl-4H-imidazo[1,5-d]thieno[2,3-b][1,4]thiazine-3-carboxylic acid

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Technology Process of 7-benzyl-4H-imidazo[1,5-d]thieno[2,3-b][1,4]thiazine-3-carboxylic acid

There total 2 articles about 7-benzyl-4H-imidazo[1,5-d]thieno[2,3-b][1,4]thiazine-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 479638-66-9
7-benzyl-4H-imidazo[1,5-d]thieno[2,3-b][1,4]thiazine-3-carboxylate

: 479638-73-8
7-benzyl-4H-imidazo[1,5-d]thieno[2,3-b][1,4]thiazine-3-carboxylic acid

Guidance literature:: With sodium hydroxide; In ethanol; water; at 85 ℃; for 2h;
DOI:10.1002/jhet.5570390407

Reference yield:

: 213402-49-4
6-benzyl-2,3-dihydro-1H-thieno[2,3-b][1,4]thiazine-2-one

: 479638-73-8
7-benzyl-4H-imidazo[1,5-d]thieno[2,3-b][1,4]thiazine-3-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: t-BuOK / tetrahydrofuran / 0.5 h / -40 - 20 °C

1.2: diethyl chlorophosphate / tetrahydrofuran / 1 h / -50 - -30 °C

1.3: 56 percent / t-BuOK / tetrahydrofuran / 1.92 h / -78 - -20 °C

2.1: 95 percent / NaOH / ethanol; H₂O / 2 h / 85 °C

With sodium hydroxide; potassium tert-butylate; In tetrahydrofuran; ethanol; water;
DOI:10.1002/jhet.5570390407

Reference yield: 60.0%

: 5619-04-5
methyl 2-amino-3-hydroxypropanoate hydrochloride

: 479638-73-8
7-benzyl-4H-imidazo[1,5-d]thieno[2,3-b][1,4]thiazine-3-carboxylic acid

: methyl 2-{[(7-benzyl-4H-imidazo[1,5-d]thieno[2,3-b][1,4]thiazine-3-yl)carbonyl]amino}-3-hydroxypropanoate

Guidance literature:: 7-benzyl-4H-imidazo[1,5-d]thieno[2,3-b][1,4]thiazine-3-carboxylic acid; With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 20 - 55 ℃; for 3h;

methyl 2-amino-3-hydroxypropanoate hydrochloride; With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 96h;
DOI:10.1002/jhet.5570390407