thexyldimethylsilyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside

Base Information

Chemical Name:thexyldimethylsilyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside
CAS No.:220734-53-2
Molecular Formula:C₃₅H₄₇N₃O₅Si
Molecular Weight:617.861
Hs Code.:

Synonyms:thexyldimethylsilyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside

Suppliers and Price of thexyldimethylsilyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of thexyldimethylsilyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of thexyldimethylsilyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside

There total 1 articles about thexyldimethylsilyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 67373-56-2
chlorodimethyl(1,1,2-trimethylpropyl)silane

: 79781-69-4
2-azido-3,4,6-tri-O-benzyl-2-deoxy-D-galactopyranose

: 220734-53-2
thexyldimethylsilyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside

Guidance literature:: With 1H-imidazole; In dichloromethane; for 1h;
DOI:10.1021/jo015840q

Reference yield:

: 220734-53-2
thexyldimethylsilyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside

: (2S,3R,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-tetrahydro-pyran-3-ylamine

Guidance literature:: With sodium tetrahydroborate; nickel dichloride; In ethanol;
DOI:10.1016/S0040-4039(98)02579-9

Reference yield:

: 220734-53-2
thexyldimethylsilyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside

: 220734-67-8
thexyldimethylsilyl 3,4,6-tri-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / NiCl₂*6H₂O / ethanol / 1 h / 20 °C

2: 1.2 g / Et₃N / CH₂Cl₂ / 0.25 h / 20 °C

With sodium tetrahydroborate; triethylamine; nickel dichloride; In ethanol; dichloromethane;
DOI:10.1021/jo015840q