(4S,4'S)-3,3'-((2R,6R)-1,7-dioxo-2,6-diethyl-4-methylene-1,7-heptanediyl)bis(4-benzyl)-2-oxazolidinone

Base Information

Chemical Name:(4S,4'S)-3,3'-((2R,6R)-1,7-dioxo-2,6-diethyl-4-methylene-1,7-heptanediyl)bis(4-benzyl)-2-oxazolidinone
CAS No.:1180517-04-7
Molecular Formula:C₃₂H₃₈N₂O₆
Molecular Weight:546.664
Hs Code.:

Synonyms:(4S,4'S)-3,3'-((2R,6R)-1,7-dioxo-2,6-diethyl-4-methylene-1,7-heptanediyl)bis(4-benzyl)-2-oxazolidinone

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Chemical Property of (4S,4'S)-3,3'-((2R,6R)-1,7-dioxo-2,6-diethyl-4-methylene-1,7-heptanediyl)bis(4-benzyl)-2-oxazolidinone

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Technology Process of (4S,4'S)-3,3'-((2R,6R)-1,7-dioxo-2,6-diethyl-4-methylene-1,7-heptanediyl)bis(4-benzyl)-2-oxazolidinone

There total 1 articles about (4S,4'S)-3,3'-((2R,6R)-1,7-dioxo-2,6-diethyl-4-methylene-1,7-heptanediyl)bis(4-benzyl)-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 17616-43-2
3-iodo-2-(iodomethyl)-1-propene

: 111292-87-6,143097-11-4,112459-79-7
(S)-4-benzyl-3-butyryloxazolidin-2-one

: 1180517-04-7
(4S,4'S)-3,3'-((2R,6R)-1,7-dioxo-2,6-diethyl-4-methylene-1,7-heptanediyl)bis(4-benzyl)-2-oxazolidinone

: 90719-32-7
(S)-4-Benzyl-2-oxazolidinone

Guidance literature:: (S)-4-benzyl-3-butyryloxazolidin-2-one; With sodium hexamethyldisilazane; In tetrahydrofuran; at -55 ℃; Inert atmosphere;

3-iodo-2-(iodomethyl)-1-propene; In tetrahydrofuran; at -55 ℃; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo901203s

Reference yield:

: 1180517-04-7
(4S,4'S)-3,3'-((2R,6R)-1,7-dioxo-2,6-diethyl-4-methylene-1,7-heptanediyl)bis(4-benzyl)-2-oxazolidinone

: C₃₂H₃₉IN₂O₇

Guidance literature:: With water; iodine; In tetrahydrofuran; at 20 ℃; for 36h; Inert atmosphere;
DOI:10.1021/jo901203s

Reference yield:

: 1180517-04-7
(4S,4'S)-3,3'-((2R,6R)-1,7-dioxo-2,6-diethyl-4-methylene-1,7-heptanediyl)bis(4-benzyl)-2-oxazolidinone

: 1180517-06-9
(S)-3-((R)-2-(((2S,4R)-4-ethyltetrahydro-2-(iodomethyl)-5-oxofuran-2-yl)methyl)butanoyl)-4-benzyloxazolidin-2-one

: 1180517-15-0
(S)-3-((R)-2-(((2R,4R)-4-ethyltetrahydro-2-(iodomethyl)-5-oxofuran-2-yl)methyl)butanoyl)-4-benzyloxazolidin-2-one

Guidance literature:: With iodine; sodium hydrogencarbonate; In acetonitrile; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo901203s