Technology Process of C60H40BN3O
There total 7 articles about C60H40BN3O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C13H13NO; 1-ethynylpyrene;
With
ethylmagnesium bromide;
In
tetrahydrofuran;
at 50 ℃;
for 2h;
Inert atmosphere;
C29H19BF2N2;
In
tetrahydrofuran;
at 25 - 70 ℃;
for 16h;
Inert atmosphere;
DOI:10.1021/jo200246q
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: water; potassium carbonate / tetrahydrofuran; methanol / 1 h
2.1: ethylmagnesium bromide / tetrahydrofuran / 2 h / 50 °C / Inert atmosphere
2.2: 16 h / 25 - 70 °C / Inert atmosphere
With
ethylmagnesium bromide; water; potassium carbonate;
In
tetrahydrofuran; methanol;
DOI:10.1021/jo200246q
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ammonium hydroxide / methanol; water; acetic acid / 24 h / 20 °C
2.1: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere
3.1: ethylmagnesium bromide / tetrahydrofuran / 2 h / 50 °C / Inert atmosphere
3.2: 16 h / 25 - 70 °C / Inert atmosphere
With
ammonium hydroxide; boron trifluoride diethyl etherate; ethylmagnesium bromide; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; dichloromethane; water; acetic acid;
DOI:10.1021/jo200246q