N-(tert-butoxycarbonyl)-D-2-(p-hydroxyphenyl)glycinylsarcosine ethyl ester

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-D-2-(p-hydroxyphenyl)glycinylsarcosine ethyl ester
CAS No.:1197196-35-2
Molecular Formula:C₁₈H₂₆N₂O₆
Molecular Weight:366.414
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-D-2-(p-hydroxyphenyl)glycinylsarcosine ethyl ester

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Chemical Property of N-(tert-butoxycarbonyl)-D-2-(p-hydroxyphenyl)glycinylsarcosine ethyl ester

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Technology Process of N-(tert-butoxycarbonyl)-D-2-(p-hydroxyphenyl)glycinylsarcosine ethyl ester

There total 1 articles about N-(tert-butoxycarbonyl)-D-2-(p-hydroxyphenyl)glycinylsarcosine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13200-60-7
Sarcosine ethyl ester

: 27460-85-1
N-(tert-butoxycarbonyl)-D-(4-hydroxyphenyl)glycine

: 1197196-35-2
N-(tert-butoxycarbonyl)-D-2-(p-hydroxyphenyl)glycinylsarcosine ethyl ester

Guidance literature:: With triethylamine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In dichloromethane; ethyl acetate; at 0 - 20 ℃;
DOI:10.3987/COM-09-11762

Reference yield: 81.0%

: 1197196-35-2
N-(tert-butoxycarbonyl)-D-2-(p-hydroxyphenyl)glycinylsarcosine ethyl ester

: 1197196-36-3
cyclo[D-2-(p-hydroxyphenyl)glycinylsarcosine]

Guidance literature:: N-(tert-butoxycarbonyl)-D-2-(p-hydroxyphenyl)glycinylsarcosine ethyl ester; With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃;

With triethylamine; In 2-methyl-propan-1-ol; 1,3,5-trimethyl-benzene; at 110 ℃; for 11h;

Large scale reaction;
DOI:10.3987/COM-09-11762