1-(phenylsulfonyl)-2-oxo-3-(2-propen-1-yl)-1,2,3,4-tetrahydronaphthalene

Base Information

Chemical Name:1-(phenylsulfonyl)-2-oxo-3-(2-propen-1-yl)-1,2,3,4-tetrahydronaphthalene
CAS No.:96964-64-6
Molecular Formula:C₁₉H₁₈O₃S
Molecular Weight:326.416
Hs Code.:

Synonyms:1-(phenylsulfonyl)-2-oxo-3-(2-propen-1-yl)-1,2,3,4-tetrahydronaphthalene

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Chemical Property of 1-(phenylsulfonyl)-2-oxo-3-(2-propen-1-yl)-1,2,3,4-tetrahydronaphthalene

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Technology Process of 1-(phenylsulfonyl)-2-oxo-3-(2-propen-1-yl)-1,2,3,4-tetrahydronaphthalene

There total 4 articles about 1-(phenylsulfonyl)-2-oxo-3-(2-propen-1-yl)-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 88116-07-8
2-Allyl-4-benzenesulfonyl-3-oxo-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid ethyl ester

: 96964-64-6
1-(phenylsulfonyl)-2-oxo-3-(2-propen-1-yl)-1,2,3,4-tetrahydronaphthalene

Guidance literature:: With dimethyl sulfoxide; at 60 - 70 ℃; for 1h;
DOI:10.1021/jo00218a022

Reference yield:

: 2049-80-1
(2-propenyl)propanedioic acid diethyl ester

: 96964-64-6
1-(phenylsulfonyl)-2-oxo-3-(2-propen-1-yl)-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / tetrahydrofuran / 0.5 h / Ambient temperature

2: 82 percent / tetrahydrofuran / 0.5 h / Ambient temperature

3: 61 percent / DMSO / 1 h / 60 - 70 °C

With sodium hydride; dimethyl sulfoxide; In tetrahydrofuran;
DOI:10.1021/jo00218a022

Reference yield:

: 88116-02-3
1-bromomethyl-2-[(phenylsulfonyl)methyl]benzene

: 96964-64-6
1-(phenylsulfonyl)-2-oxo-3-(2-propen-1-yl)-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / tetrahydrofuran / 0.5 h / Ambient temperature

2: 82 percent / tetrahydrofuran / 0.5 h / Ambient temperature

3: 61 percent / DMSO / 1 h / 60 - 70 °C

With sodium hydride; dimethyl sulfoxide; In tetrahydrofuran;
DOI:10.1021/jo00218a022