dithiocarbonic acid S-{[tert-butyl-(2,6-dichloro-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

Base Information

• Chemical Name: dithiocarbonic acid S-{[tert-butyl-(2,6-dichloro-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester
• CAS No.: 864365-03-7
• Molecular Formula: C₁₈H₂₅Cl₂NO₂S₂
• Molecular Weight: 422.44

Synonyms:dithiocarbonic acid S-{[tert-butyl-(2,6-dichloro-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

Chemical Property of dithiocarbonic acid S-{[tert-butyl-(2,6-dichloro-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

Chemical Property:

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Technology Process of dithiocarbonic acid S-{[tert-butyl-(2,6-dichloro-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester

There total 3 articles about dithiocarbonic acid S-{[tert-butyl-(2,6-dichloro-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

N-tert-butyl-2-chloro-N-(2,6-dichloro-phenyl)-acetamide (864364-95-4) + sodium O-neopentyl xanthate salt → dithiocarbonic acid S-{[tert-butyl-(2,6-dichloro-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester (864365-03-7)

Guidance literature:

In acetonitrile; for 6h; Heating;

DOI:10.1021/ol051568l

Reference yield:

tert-butyl-(2,6-dichloro-phenyl)-amine (864365-11-7) → dithiocarbonic acid S-{[tert-butyl-(2,6-dichloro-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester (864365-03-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / N,N-dimethylaniline / 1,2-dichloro-ethane / Heating

2: 87 percent / acetonitrile / 6 h / Heating

With N,N-dimethyl-aniline; In 1,2-dichloro-ethane; acetonitrile;

DOI:10.1021/ol051568l

Reference yield:

2,6-Dichloroaniline (608-31-1) → dithiocarbonic acid S-{[tert-butyl-(2,6-dichloro-phenyl)-carbamoyl]-methyl} ester O-(2,2-dimethyl-propyl) ester (864365-03-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 66 percent / BF₃*OEt₂ / cyclohexane / 20 °C

2: 94 percent / N,N-dimethylaniline / 1,2-dichloro-ethane / Heating

3: 87 percent / acetonitrile / 6 h / Heating

With boron trifluoride diethyl etherate; N,N-dimethyl-aniline; In cyclohexane; 1,2-dichloro-ethane; acetonitrile;

DOI:10.1021/ol051568l

upstream raw materials:

N-tert-butyl-2-chloro-N-(2,6-dichloro-phenyl)-acetamide

tert-butyl-(2,6-dichloro-phenyl)-amine

2,6-Dichloroaniline

Downstream raw materials:

1,2-bis-(2,6-dichlorophenyl)ethane

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