Acetic acid 12-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-12-oxo-dodecyl ester

Base Information

Chemical Name:Acetic acid 12-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-12-oxo-dodecyl ester
CAS No.:104966-93-0
Molecular Formula:C₂₃H₃₆O₆
Molecular Weight:408.535
Hs Code.:

Synonyms:Acetic acid 12-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-12-oxo-dodecyl ester

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Chemical Property of Acetic acid 12-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-12-oxo-dodecyl ester

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Technology Process of Acetic acid 12-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-12-oxo-dodecyl ester

There total 4 articles about Acetic acid 12-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-12-oxo-dodecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 947-05-7
oxacyclotridecan-2-one

: 104966-93-0
Acetic acid 12-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-12-oxo-dodecyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: NaOH / methanol / 5 h / Heating

2: 60 °C

3: PCl₅ / CH₂Cl₂ / 2 h / 25 °C

4: AlCl₃ / 1,2-dichloro-ethane / 5 degC, 2 h; 20 degC, 70 h

With sodium hydroxide; aluminium trichloride; phosphorus pentachloride; In methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1248/cpb.33.4422

Reference yield:

: 100912-48-9
12-acetoxydodecanoic acid

: 104966-93-0
Acetic acid 12-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-12-oxo-dodecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: PCl₅ / CH₂Cl₂ / 2 h / 25 °C

2: AlCl₃ / 1,2-dichloro-ethane / 5 degC, 2 h; 20 degC, 70 h

With aluminium trichloride; phosphorus pentachloride; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1248/cpb.33.4422

Reference yield:

: 51828-75-2
Sodium; 12-hydroxy-dodecanoate

: 104966-93-0
Acetic acid 12-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-12-oxo-dodecyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 60 °C

2: PCl₅ / CH₂Cl₂ / 2 h / 25 °C

3: AlCl₃ / 1,2-dichloro-ethane / 5 degC, 2 h; 20 degC, 70 h

With aluminium trichloride; phosphorus pentachloride; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1248/cpb.33.4422