tert-butyl 2-((5-(2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yloxy)pentyl)(2-mercaptoethyl)amino)-N-(2-mercaptoethyl)acetamide

Base Information

Chemical Name:tert-butyl 2-((5-(2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yloxy)pentyl)(2-mercaptoethyl)amino)-N-(2-mercaptoethyl)acetamide
CAS No.:1384435-33-9
Molecular Formula:C₂₆H₃₆N₄O₃S₂
Molecular Weight:516.729
Hs Code.:

Synonyms:tert-butyl 2-((5-(2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yloxy)pentyl)(2-mercaptoethyl)amino)-N-(2-mercaptoethyl)acetamide

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Chemical Property of tert-butyl 2-((5-(2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yloxy)pentyl)(2-mercaptoethyl)amino)-N-(2-mercaptoethyl)acetamide

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Technology Process of tert-butyl 2-((5-(2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yloxy)pentyl)(2-mercaptoethyl)amino)-N-(2-mercaptoethyl)acetamide

There total 6 articles about tert-butyl 2-((5-(2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yloxy)pentyl)(2-mercaptoethyl)amino)-N-(2-mercaptoethyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.3%

: 1384435-32-8
N-(2-(4-methoxybenzylthio)ethyl)-2-((2-(4-methoxybenzylthio)ethyl)(5-(2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yloxy)pentyl)amino)acetamide

: 1384435-33-9
tert-butyl 2-((5-(2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yloxy)pentyl)(2-mercaptoethyl)amino)-N-(2-mercaptoethyl)acetamide

Guidance literature:: With methanesulfonic acid; methoxybenzene; trifluoroacetic acid; at 0 - 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2012.05.010

Reference yield:

: 1383563-18-5
2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-ol

: 1384435-33-9
tert-butyl 2-((5-(2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yloxy)pentyl)(2-mercaptoethyl)amino)-N-(2-mercaptoethyl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 90 °C

2: potassium carbonate / acetonitrile / 90 °C

3: methanesulfonic acid; methoxybenzene; trifluoroacetic acid / 1 h / 0 - 20 °C

With methanesulfonic acid; potassium carbonate; methoxybenzene; trifluoroacetic acid; In acetonitrile;
DOI:10.1016/j.bmcl.2012.05.010

Reference yield:

: 1383563-17-4
4-(5-methoxybenzo[d]oxazol-2-yl)-N,N-dimethylbenzenamine

: 1384435-33-9
tert-butyl 2-((5-(2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yloxy)pentyl)(2-mercaptoethyl)amino)-N-(2-mercaptoethyl)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: boron tribromide / dichloromethane / 3 h / -78 °C

2: potassium carbonate / acetonitrile / 90 °C

3: potassium carbonate / acetonitrile / 90 °C

4: methanesulfonic acid; methoxybenzene; trifluoroacetic acid / 1 h / 0 - 20 °C

With methanesulfonic acid; boron tribromide; potassium carbonate; methoxybenzene; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2012.05.010