methyl 2,3,6-trideoxy-2-fluoro-3-iodo-4-O-p-nitrobenzoyl-α-L-talopyranoside

Base Information

Chemical Name:methyl 2,3,6-trideoxy-2-fluoro-3-iodo-4-O-p-nitrobenzoyl-α-L-talopyranoside
CAS No.:211993-25-8
Molecular Formula:C₁₄H₁₅FINO₆
Molecular Weight:439.179
Hs Code.:

Synonyms:methyl 2,3,6-trideoxy-2-fluoro-3-iodo-4-O-p-nitrobenzoyl-α-L-talopyranoside

Suppliers and Price of methyl 2,3,6-trideoxy-2-fluoro-3-iodo-4-O-p-nitrobenzoyl-α-L-talopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 2,3,6-trideoxy-2-fluoro-3-iodo-4-O-p-nitrobenzoyl-α-L-talopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 2,3,6-trideoxy-2-fluoro-3-iodo-4-O-p-nitrobenzoyl-α-L-talopyranoside

There total 6 articles about methyl 2,3,6-trideoxy-2-fluoro-3-iodo-4-O-p-nitrobenzoyl-α-L-talopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114643-57-1
methyl 3-O-acetyl-4-O-benzyl-2,6-dideoxy-2-fluoro-α-L-idopyranoside

: 211993-25-8
methyl 2,3,6-trideoxy-2-fluoro-3-iodo-4-O-p-nitrobenzoyl-α-L-talopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: H₂ / Pd black / dioxane; H₂O; acetic acid / 1 h / Ambient temperature

2: 97 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / Ambient temperature

3: 98 percent / Zemplen deacetylation / methanol

4: 94 percent / pyridine / CH₂Cl₂ / 1 h

5: NaI / dimethylformamide / 3 h / 90 °C

6: 4-dimethylaminopyridine / dimethylformamide / 2.5 h / Ambient temperature

With pyridine; dmap; hydrogen; pyridinium p-toluenesulfonate; sodium iodide; palladium; In 1,4-dioxane; methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(98)00026-3

Reference yield:

: 211993-22-5
methyl 2,6-dideoxy-2-fluoro-4-O-tetrahydropyran-2-yl-α-L-idopyranoside

: 211993-25-8
methyl 2,3,6-trideoxy-2-fluoro-3-iodo-4-O-p-nitrobenzoyl-α-L-talopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / pyridine / CH₂Cl₂ / 1 h

2: NaI / dimethylformamide / 3 h / 90 °C

3: 4-dimethylaminopyridine / dimethylformamide / 2.5 h / Ambient temperature

With pyridine; dmap; sodium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(98)00026-3

Reference yield:

: 211993-20-3
methyl 3-O-acetyl-2,6-dideoxy-2-fluoro-α-L-idopyranoside

: 211993-25-8
methyl 2,3,6-trideoxy-2-fluoro-3-iodo-4-O-p-nitrobenzoyl-α-L-talopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / Ambient temperature

2: 98 percent / Zemplen deacetylation / methanol

3: 94 percent / pyridine / CH₂Cl₂ / 1 h

4: NaI / dimethylformamide / 3 h / 90 °C

5: 4-dimethylaminopyridine / dimethylformamide / 2.5 h / Ambient temperature

With pyridine; dmap; pyridinium p-toluenesulfonate; sodium iodide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(98)00026-3